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Contents ABSTRACT ...........................................................................................................................4 INTRODUCTION.................................................................................................................5 PART I - STATE OF THE ART CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY.....................................................8 1.1 UNITS OF CONDUCTIVITY............................................................................................10 1.2 CONCEPT OF THE CELL CONSTANT ..............................................................................12 1.3 TEMPERATURE EFFECTS..............................................................................................15 1.4 POLARISATION ............................................................................................................19 1.5 TOTAL DISSOLVED SOLIDS (TDS) ..............................................................................19 1.6 ALTERNATIVE MEASUREMENT TECHNOLOGIES ..........................................................19 1.6.1 Contacting conductivity ......................................................................................19 1.6.2 Toroidal (Inductive) conductivity .......................................................................21 1.7 SOURCES OF ERROR IN MEASUREMENT ........................................................................22 1.7.1 Temperature Compensation................................................................................22 1.7.2 Improper Calibration..........................................................................................23 1.7.3 Condition of Probe..............................................................................................23 CHAPTER 2 THE INDUCTIVE CONDUCTIVITY SENSOR ..............................................................24 2.1 THE EXACT THEORY OF INDUCTIVE CONDUCTIVITY SENSORS ...................................24 2.1.1 The Single Transformer ......................................................................................25 2.1.2 The Double Transformer ....................................................................................28 2.2 THE INDUCTIVE CONDUCTIVITY CELL FOR WATER SALINITY MONITORING ..................31 2.2.1 Sensor design ......................................................................................................31 2.2.2 Sensor modelling.................................................................................................32 2.2.3 Experimental characterization ...........................................................................35 PART II - THE PROPOSAL CHAPTER 3 GENERAL DESCRIPTION OF THE WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING .................................................................................37 3.1 GENERAL ARCHITECTURE OF WIRELESS CONDUCTIVITY SENSING..............................37 3.1.1 Hardware architecture .......................................................................................37 1 3.2 GENERAL ARCHITECTURE OF OSCILLATOR .................................................................42 3.2.1 Requirements for Oscillation ..............................................................................43 3.2.2 Phase Shift in the Oscillator ...............................................................................45 3.2.3 Gain in the Oscillator .........................................................................................47 3.2.4 Effect of the Active Element (Op Amp) on the Oscillator ...................................47 3.2.5 Analysis of Oscillator Operation (Circuit) .........................................................49 3.2.6 Sine Wave Oscillator Circuits.............................................................................51 3.3 MICROCONTROLLERS DESIGNER .................................................................................53 3.3.1 Microcontrollers choice......................................................................................55 3.4 INTELLIGENT RF MODULE ...........................................................................................56 3.4.1 ‘One Way’ Easy-Radio for Transmitters & Receivers........................................57 3.4.2 ‘Two Way’ for Transceivers ...............................................................................59 3.4.3 RSSI - Received Signal Strength Indicator .........................................................62 PART III - IMPLEMENTATION CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE.......................................................63 4.1 ELECTRICAL CIRCUIT OF THE HARDWARE INDUCTIVE SENSOR INTERFACE .................64 4.1.1 Quadrature Oscillator & operational amplifier TL082C...................................66 4.1.2 Analog Multiplier - AD633 .................................................................................69 4.1.3 Low-pass Filters .................................................................................................73 4.1.4 Connectors ..........................................................................................................75 4.2 BUILDING PCB HARDWARE SENSOR INTERFACE .........................................................76 4.3 BILL OF MATERIALS 1° PCB........................................................................................78 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER..............................80 5.1 ELECTRICAL CIRCUIT OF THE NODE ............................................................................80 5.1.1 Microcontroller 18F458 .....................................................................................83 5.1.2 Temperature Sensor AD22103...........................................................................88 5.1.3 Analog input and A/D conversion.......................................................................92 5.1.4 Digital Potentiometer – AD7376 ........................................................................94 5.1.5 DIP Switch ........................................................................................................100 5.1.6 Connection PIC18F458 - RF transceiver.........................................................101 5.1.7 Antenna .............................................................................................................106 5.1.8 Voltage regulator..............................................................................................108 5.1.9 Connectors ........................................................................................................110 5.2 BUILDING PCB NODE ................................................................................................111 5.3 BILL OF MATERIALS 2° PCB......................................................................................112 5.4 ELECTRICAL CIRCUIT OF THE CCP INTERFACE ..........................................................115 5.4.1 Bridge RF transceiver - Max232 – RS232 port ...............................................117 5.4.2 Voltage regulator..............................................................................................118 5.5 BUILDING PCB MASTER SERVER ...............................................................................119 2 5.6 BILL OF MATERIALS 3° PCB......................................................................................120 PART IV - EXPERIMENTAL RESULTS CHAPTER 6 TESTING AND CHARACTERIZATION OF THE INDUCTIVE SENSOR................122 6.1 THE LOW-COST TEMPERATURE CONTROLLED SYSTEM: SYSTEM DESCRIPTION ........122 6.1.1 The container ....................................................................................................123 6.1.2 Heating/cooling thermoelectric pump ..............................................................124 6.1.3 Measuring System .............................................................................................125 6.1.4 PID controller...................................................................................................126 6.2 EXPERIMENTAL CHARACTERIZATION ........................................................................127 6.2.1 Experimental setup ...........................................................................................127 6.2.2 Experimental Characterization and Discussion ...............................................129 CONCLUSIONS ...............................................................................................................136 APPENDIX A....................................................................................................................137 MPLAB IDE...................................................................................................................137 APPENDIX B....................................................................................................................142 C18 C COMPILER ............................................................................................................142 APPENDIX C....................................................................................................................143 ALTIUM DESIGNER 6.......................................................................................................143 APPENDIX D...................................................................................................................145 EASY-RADIO SOFTWARE AND CONFIGURATION COMMAND SET ....................................145 BIBLIOGRAPHY .............................................................................................................150 3 Abstract This thesis presents the development of a conductivity sensing network based on wireless transmission. The architecture of the system includes two sensors (inductive conductivity and temperature), a first PCB (Hardware Inductive Sensor Interface) that drives the inductive sensor with a sinusoidal oscillator and extracts the DC-signal components in phase and quadrature of the inductive sensor output voltage, a second PCB where a temperature sensor, a processing and communication unit, (18F458 microcontroller), and a RF transceiver for wireless communication is mounted and a third PCB where is mounted the RF transceiver used as interface with the central control and processing unit (CCP) monitoring the data. The experimental data proves that is possible to measure the electrical conductivity of the salty water by using the projected remote system. 4 Introduction Water Quality (WQ) monitoring of rivers and seas represents an important task of life quality assessment. The main parameters associated with the water quality assessment tasks can be classified in three categories: physical parameters (temperature, pH, dissolved oxygen, turbidity, conductivity), chemical parameters (heavy metal concentration, nitrate and phosphorous concentration) and biological parameters (algae and bacteria). The WQ physical parameters, usually measured by using multiparameter measurement systems, play an important role on the chemical and biological process in the surface and ground waters. The parameters of the water analyzes are the conductivity and the temperature. In this case, the salinity of the water inside estuary, where the salty tide meets the fresh water current, may be measured by using conductivity sensors, because the electric conductivity is directly related to salt content in the water. For measuring the conductivity of electrolytic solutions, there are, in principle, two groups of sensors: 1) classical conductivity cells containing two or more electrodes; 2) inductive conductivity sensors containing one or two transformers. In the sea and rivers the presence of biological organisms and the continuous deposition of inorganic materials carry to choice the second type of sensors (inductive conductivity sensors) because the utilization of nude electrodes is especially vulnerable fouling, in fact the conductance between electrodes is very sensitive to the depositions on their surface. The inductive sensors present the advantage of a non-direct contact between the sensors elements and the medium under test [1]. This characteristic allows this type of sensor to be used for water salinity monitoring. In this work of thesis the project and construction of the first prototype of a single remote node for the measurement of the conductivity and temperature of the water based on wireless transmission will be presented. The system structure offers the possibility to add, 5 INTRODUCTION without hard investments, other water quality measuring capabilities (e.g. pH, dissolved oxygen). The remote nodes will be used to the water salinity monitoring of the Tagus river in Lisbon (Portugal) near the estuary. In Figure 1 is shown the map of the Tagus estuary. Figure 1 - Map of the Tagus estuary In the first chapter the theory and application of conductivity will be described, in particular the different type of the sensors to measure the conductivity, the temperature effect, and the sources of error in measurement. In the second chapter the inductive sensor used in this project will be described, this inductive sensor has been developed at the Instituto de Telecomunicações (it) of Lisbon, in a particular way the exact theory of inductive conductivity and the sensor design. In the third chapter the general characteristics of Conductivity Sensing Network Based On Wireless Transmission will be described with particular attention to the hardware 6 INTRODUCTION architecture as the Oscillator, Microcontrollers and the RF module used to develop the main functionalities of the Remote Water Quality Monitoring System. In the fourth chapter the project and construction of a first PCB (Printed Circuit Board) called Hardware Sensor Interface used to drive an inductive conductivity sensor for water salinity monitoring will be presented. The sensor used is an inductive conductivity sensor described in the second chapter. The PCB has the following functions: 1) driving the inductive sensor by a sinusoidal oscillator. This oscillator has two outputs with exactly equal amplitudes but with a phase difference of π/2; 2) by using multipliers and convenient signal conditioning, the amplitudes of the components in phase and of phase π/2 of the sensor output are obtained in the form of two DC-signals. In the fifth chapter the second PCB where is mounted a temperature sensor, a processing and communication unit (18F458 microcontroller) and a RF transceiver for wireless communication and a third PCB, where is mounted the RF transceiver with the PC master server for monitoring the data will be presented. In the sixth chapter the testing and the characterization of the node with the inductivity conductivity sensor mounted on the first PCB will be presented. A low cost testing bath with automated controlled temperature to characterize sensors for in-situ water quality monitoring building in IT laboratories will be used. 7 Chapter 1 Theory and Application of Conductivity Conductivity (or Electrolytic Conductivity) is defined as the ability of a substance to conduct electrical current. It is the reciprocal of the resistivity [2]. In water, it is generally used as a measure of the mineral or other ionic concentration. Conductivity is a measure of the purity of water or the concentration of ionized chemicals in water. However, conductivity is only a quantitative measurement: it responds to all ionic content and cannot distinguish particular conductive materials in the presence of others. Only ionizable materials will contribute to conductivity; materials such as sugars or oils are not conductive. In a metal conductor, electrical current is the flow of electrons and is called electronic conductance. In water, electrical current is carried by ions since electrons do not pass through water by themselves. This is electrolytic conductance. When a voltage is applied between two inert electrodes immersed in a solution, any ions between them will be attracted by the electrode with the opposite charge. Ions will move between electrodes and produce a current depending on the electrical resistance of the solution. This is the basis of conductivity measurement - an application of Ohm’s law (show Figure 1.1). For high purity waters, it is common to express conductivity as its reciprocal, resistivity. 8 CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY Figure 1.1 - Using Ohms Law , V= iR and knowing conductivity G = 1/R then G can be determined as G= 1/R = i/V To prevent altering the sample by major ionic movement and electrochemical reaction at the electrodes, alternating current is always used for measurement. With AC the polarity changes frequently enough that ions do not move or react significantly. Measuring systems must control the voltage, frequency and current density to minimize errors due to electrode polarization and capacitance. Modern instrumentation may change one or more of these variables automatically, depending on the conductivity range being measured. In the chemical water treatment field our interest is in measuring the conductivity of waters which consist of ionic compounds dissolved in the water. This conductivity is quite easily measured by electronic means and this offers a simple test or control level which can tell much about the quality of the water. Conductivity of very dilute solutions can be calculated from physical chemistry data based on Equation 1.1 which sums the conductivity contribution of all ions in the solution [4]. σ = ρ * Σ (λi * ci) σ = conductivity ρ = density of water λi = equivalent ionic conductance of ion ‘i’ c i = concentration of ion ‘i’ 9 (1.1) CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY 1.1 Units of Conductivity The basic unit of resistance is the ohm, - conductance is the reciprocal of resistance and its basic unit is the siemens, formerly called the mho [2]. In discussions of bulk material it is convenient to talk of its specific conductance, or more commonly called its conductivity. Conductivity is the conductance as measured between the opposite faces of a 1- cm cube of the Material (show Figure 1.2) . Figure 1.2 – cell constant = 1 cm electrode spacing divided by 1 cm2 cross-sectional area of sample This measurement has units of Siemens/cm. More common in water treatment the units μS/cm (microsiemens) and mS/cm (millisiemens) are used as they are more meaningful. The corresponding terms for specific resistance (or resistivity) is ohm-cm, megohm-cm and kilohm-cm. Measurement Resistance Conductance Resistivity Conductivity Application Electrical circuit Electrical circuit High purity water Most water samples Units Ohm (Ω) ohm-1 (Ω-1) = siemens (S) = mho (now obsolete) Ohm⋅cm (Ω⋅cm) siemens/cm (S/cm) = mhos/cm (now obsolete), siemens/m (S/m)* * Most users employ units of S/cm. However, SI conductivity units used in some parts of the world are S/m which can easily be confused. 1 S/cm = 100 S/m. Review the following tables for typical conductivity of the water at the temperature of 25°C [5] 10 CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY table 1.1 – Typical conductivity of the water at the temperature of 25 °C A conductivity measurement responds to any and all ions present in a solution. A solution cannot be identified, or its concentration known, from conductivity alone (see Figure 1.3). In certain cases, the concentration of an electrolyte in solution can be determined by conductivity if the composition of the solution is known [6]. 11 CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY Figure 1.3 - A solution cannot be identified from conductivity alone 1.2 Concept of the cell constant In theory, a conductivity measuring cell is formed by two 1-cm square surfaces spaced 1cm apart. Cells of different physical configuration are characterized by their cell constant, Kc. This cell constant (Kc) is a function of the electrode areas, the distance between the electrodes and the electrical field pattern between the electrodes [3]. A cell for measuring conductivity may be made up as shown in the Figure 1.4, it is made of insulating material except for the opposite faces A and B which are made of metal. If it is filled with a conductivity solution L, the conductance measured between the faces A and B is the following: G = L A/ l where G = conductance in Siemens L = Conductivity in Siemens/cm l = distance in cm between the electrodes or faces A and B A = surface in cm2 perpendicular to the flow of current. 12 CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY Figure 1.4 - A cell for measuring conductivity The corresponding equation for the resistance is: R = ρ l /A where R = resistance in ohm ρ = resistivity in ohm*cm l = distance in cm between the electrodes A = surface in cm2 perpendicular to the flow of current. The term l /A is defined as Kc, the cell constant of resistivity, and its measuring unit is the cm-1. Conductivity Cell Constant = −1 Length 1 cm = = 1cm 2 Area 1 cm The cell constant of the resistivity is used for all the applications, irrespective of whether conductivity or resistivity is being used: the result is G = L/Kc or KcG = L For example, for an observed conductance reading of 200 µS using a cell with Kc 0. 1, the conductivity value is 200 x 0. 1 = 20 µS/cm [5]. As the dimensions of the cell change, the cell constant varies with the ratio l /A (show Figure 1.5). 13 CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY (a) (b) Figure 1.5 – (a) 0.1 constant; (b) 10.0 constant Cell constants other than 1 cm-1 may be used as long as the measuring instrument readout is normalized accordingly. A lower cell constant sensor is needed to enable the measuring instrument to make accurate measurements in low conductivity (high resistivity) samples. Higher cell constants are needed to measure in high conductivity samples. The exact requirements depend on the measuring instrument. In a simplified approach, the cell constant is defined as the ratio of the distance between the electrodes, l, to the electrode area, A. This however neglects the existence of a fringefield effect, which affects the electrode area by the amount AR. Therefore Kc = l/(A + AR). Because it is normally impossible to measure the fringe-field effect and the amount of AR to calculate the cell constant, Kc, the actual Kc of a specific cell is determined by a comparison measurement of a standard solution of known electrolytic conductivity. The most commonly used standard solution for calibration is 0.01 M KCl. This solution has a conductivity of 1412 µS/cm at 25oC In summary, the calibration of a conductivity probe is to compensate for the fact that: • Kc is not specifically known • Kc changes as the electrode ages Calibration simply adjusts the measured reading to the true value at a specified temperature [3]. In order to produce a measuring signal acceptable to the conductivity meter, it is highly important that the user choose a conductivity electrode with a cell constant appropriate for 14 CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY his sample. The table below lists the optimum conductivity range for cells with different cell constants. Cell Constant Optimum Conductivity Range 0.01 0.055 - 20 μS/cm 0.1 0.5 - 200 μS/cm 1.0 0.01 - 2 mS/cm 10.0 1 - 200 mS/cm table 1.2 – Lists the optimum conductivity range for cells with different cell constants 1.3 Temperature Effects Conductivity is affected by temperature since water becomes less viscous and ions can move more easily at higher temperatures. Conventionally, conductivity measurements are referenced to 25 °C though occasionally a 20 °C reference is used [3]. The variation with temperature is apparent in Equation 1.1 since λi, and to a lesser degree, ρ are temperature dependent. The conductivity of most ions increase in conductivity by about 2.2% of their value per °C which allows for simple temperature compensation. This is suitable for most mid-range conductivity measurements. Very low and very high conductivity samples require special handling of temperature effects. In moderately and highly conductive solutions, this increase can be compensated for using a linear equation involving a temperature coefficient (α), which is the percent increase in conductivity per degree centigrade (see Figure 1.6). The degree to which temperature affects conductivity varies from solution to solution and can be calculated using the following formula: CT = CTcal [1 + α(T-Tcal)] where: 15 (1.2) CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY CT = conductivity at any temperature T in °C; CTcal = conductivity at calibration temperature Tcal in °C; α = temperature coefficient of solution at Tcal in °C. The temperature coefficients of the following electrolytes generally fall in the ranges shown below: Substance at 25°C Alpha (α) Acids 1.0 - 1.6%/°C Bases 1.8 - 2.2%/°C Salts 2.2 - 3.0%/°C Fresh water 2.0%/°C For example, by definition, temperature compensated conductivity of a solution is the conductivity which that solution exhibits at the reference temperature. This temperature is chosen to be either 25 oC or 20 oC. A measurement made at reference temperature, therefore, needs no compensation. Generally for most aqueous samples, a coefficient of 2.1% per degree Celcius is used in temperature compensation, with the apparent value being 2.1% high for each degree C above 25 oC or conversely the apparent value being 2.1% low for each temperature for measurement is 25 oC. Using the formula (1.2): CT = C25 [1 + 0.021 (T - 25)] To determine that α of other solutions, simply measure conductivity at a range of temperatures and graph the change in conductivity versus the change in temperature. Divide the slope of the graph by CTcal to get α. 16 CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY Figure 1.6 - Temperature Compensation for Conductivity Increase with Temperature For example in Figure 1.6 is show the conductivity vs temperature for a generic solution [6]. To calculate the temperature coefficient (α) to be input into a conductivity analyzer, simply: 1. Divide the temperature slope(s): ⎡ 60-30mS/cm ⎤ S= ⎢ ⎥⎦ = 1.20 50 - 25 °C ⎣ 2. By the conductivity at 25°C, C(25°C): S 1.2 = = 0.040 o C(25 C) 30 3. and multiply by 100: α = 100 (.040) = 4.0% All meters have either fixed or adjustable automatic temperature compensation referenced to a standard temperature - usually 25°C. Most meters with fixed temperature compensation use a a of 2%/°C (the approximate a of NaCl solutions at 25°C). Meters with adjustable temperature compensation let you to adjust the a to more closely match the a of your measured solution. A very modern technique uses a microprocessor and an associated "look up" table which contains the temperature response of the solution. The solution temperature is measured 17 CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY and converted to digital form, from this information and data in the "look up" table a very accurate temperature compensation can be derived. Note the two following examples to explain the effect and compensation of the fringe-field effect and temperature. Example #1 - Manual Temperature Compensation: An analyst wishes to calibrate a conductivity probe and measure an unknown sample. The conductivity probe is specified to have a cell constant of 1.0. The analyst is calibrating in a 0.01 M KCI (EC = 1412 µS/cm at 25oC) solution at a temperature of 22oC. Automatic temperature compensation (ATC) is not available. 1. 2. Determine the conductivity of the 0.01 M KCI at 22oC. o EC KCI 22oC = 1412[l + 0.021(22-25)] o EC KCI 22oC = 1412 [0.937] o EC KCI 22oC = 1323 µS/cm Immerse the conductivity probe into the standard and adjust the value to 1323 µS/cm. adjustment being made is compensating for the difference the specified cell constants and the true cell constant. 3. The analyst now measures an unknown sample whose temperature is at 19oC and obtains a value of 967 µS/cm. How is this value adjusted to 25oC 967 µS/CM = C25[1 + 0.021(19-25)] C25 = 967 µS / [1 + 0.021(19-25)] C25 = 967 µS / [1 + 0.021(-6)] C25 = 967 µS / 0.874 C25 = 1106 µS/cm Example #2 - Automatic Temperature Compensation: An analyst wishes to calibrate the conductivity probe and measure a sample. The conductivity probe is specified to have a cell constant of 1.0. The analyst is calibrating in a 0.01 M KCI (EC = 1412 µS/cm at 25oC) solution at a temperature of 22oC. Automatic temperature compensation (ATC) at 25oC is available. 1. Immerse the conductivity probe into the standard and adjust the value to 1412 µS/cm. Any adjustment being made is compensating for the difference between the specified cell constants and the true cell constant. NOTE: On most modern instrumentation, the true temperature is displayed along with the temperature compensated conductivity value. In this case the display would show a conductivity of 1412 µS/cm and of 22oC. 2. Once the electrode has been calibrated, it is cleaned, placed into the unknown sample at 19oC. Once temperature is stable, the correct conductivity value (1106) µS is displayed 18 CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY 1.4 Polarisation Polarisation can cause formation of gas at metallic surfaces even though high frequency AC is used in measurement, the effect can take place in the half cycle of one polarity. Another reason is a depletion of anions or cations around the electrode due to the charge build up. Polarisation is an insidious effect in that conductivity readings can be lower than the true value but by an unknown amount and a reading is obtained from the instrument with no indication that it is incorrect. Similar effects are noted if grease or oil are present in the solution, or if the electrodes are fouled or scaled in any way. Polarisation can be reduced by using high frequency AC, keeping the current density low by the correct choice of cell constant and by making surfaces rough such as graphite, and by operating in conductivities of less that 30,000 μS/cm, and in the case of fouling, by removal of the sensor and cleaning frequently [2]. 1.5 Total Dissolved Solids (TDS) TDS is sometimes inferred from conductivity and is reported in units of parts per million. However, the relationship of conductivity and concentration is not standardized and to be meaningful, should be specified whenever TDS units are used. Typical conversions are based on sodium chloride (which may also be called salinity) at approximately 0.5 ppm TDS per μS/cm. Alternatively, a “natural water” mineral composition including bicarbonates would have a conversion of 0.6 – 0.7 ppm TDS per μS/cm. Conversions may also be slightly non-linear with concentration. 1.6 Alternative Measurement Technologies 1.6.1 Contacting conductivity In Figure 1.1 and its description above refer to the conventional two-electrode sensor and measurement technique. Most practical cells do not use the parallel plate electrode arrangement of Figure 1.1. They have greater durability and allow more convenient installation with other arrangements. 19 CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY For example, typical pure water sensors for on-line measurement use concentric electrodes that maintain the spacing and geometry for 0.01 to 0.1/cm constant. A variety of twoelectrode process conductivity sensors is illustrated in Figure 1.7. Figure 1.7 – Conventional two-electrode conductivity sensors: 0.1 cm-1in retractable housing,0.1 cm-1in flow chamber, sanitary 0.1 cm-1, 10cm-1insertion, 50-1cm insertion, long 0.1cm-1insertion, short 0.1 cm-1insertion. Four-electrode conductivity measurement uses a sensor incorporating four electrodes. It is useful for highly conductive and/or dirty water samples which would foul the surfaces or plug the narrow passages of conventional high constant two-electrode sensors [4]. Four-electrode measurement applies AC through the sample via two outer drive electrodes as shown in Figure 1.8. V Figure 1.8 – Four-electrode conductivity measurement 20 CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY These electrodes may become fouled and the circuit will compensate to maintain the AC current level constant. Two inner measuring electrodes are used to sense the voltage drop through the portion of solution between them. The circuit makes a high impedance AC voltage measurement, drawing negligible current and making it much less affected by additional resistance due to fouling of the measuring electrode surfaces. Sensors for four electrode conductivity measurement are shown in Figure 1.9. Figure 1.9 – Four-electrode Conductivity Sensors 1.6.2 Toroidal (Inductive) conductivity Inductive (also known as non-contact, electrodeless or toroidal) conductivity measurement is made without any direct electrical contact with the sample. The sensor consists of two parallel coils sealed within a doughnut-shaped insulated probe as shown in Figures 1.10 and 1.11. A transmitting coil generates a magnetic alternating field that induces an electric voltage in a liquid. The ions present in the liquid enable a current flow that increases with increasing ion concentration. The ionic concentration is then proportional to the conductivity. The current in the liquid generates a magnetic alternating field in the receiving coil. The resulting current induced in the receiving coil is measured and used to determine the conductivity value of the solution. Advantages to this type of cell are: • No polarization • Reduced maintenance and resistance to chemical attack • Complete galvanic separation of measurement from medium (eliminates ground loss) 21 CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY Figure 1.10 – Inductive Conductivity Measurement Figure 1.11 – Inductive Conductivity Measurement Equipment 1.7 Sources of error in measurement 1.7.1 Temperature Compensation Since many conductivity probes now include a thermistor for ATC it is important to determine if the thermistor reading is accurate at the temperatures that samples are being measured. If not, then the automatic temperature corrected value will be inaccurate. Compare the measured value from the thermistor with that of a quality laboratory 22 CHAPTER 1 THEORY AND APPLICATION OF CONDUCTIVITY thermometer. If the values differ significantly, contact the manufacturer as to the defect or consider manual temperature compensation. 1.7.2 Improper Calibration Too often, calibration standards have been sitting around a laboratory for extended periods. Standards should be fresh and known to be correct within at least ± 1% before attempting a calibration. Since the conductometric response is not perfectly linear at all ranges it is best to calibrate the probe in the same magnitude of range as the samples being measured. In other words don't calibrate your conductivity probe in a 100 µS/cm standard if your samples are typically in the >1000 µS/cm range. Standard conductivity solutions: Conductivity (mS/cm)1 0.147 1.413 2.767 6.668 KCI Concentration 0.001 N 0.010 N 0.020 N 0.050 N 1 temperature KCl solutions 250C 1.7.3 Condition of Probe Probes can become inaccurate when they become coated with interfering substances on the probe element. During normal use, rinse the probe thoroughly with laboratory grade water between each measurement. This will help to minimize the buildup of the coating substances. If the probe needs cleaning first try ethanol which is good for removing most organics. If this isn't successful, clean the probe with a strong detergent solution. Rinse thoroughly with demineralized water. The cells may occasionally need replatinization to refresh the cell plates and return them back to the original cell constant. The cell constant changes when the platinum black layer becomes partially removed or contaminated. Follow the manufacturer's directions on this procedure [3]. 23 Chapter 2 The Inductive Conductivity Sensor Besides temperature and pressure, conductivity is among the most relevant parameters characterizing the physical (thermodynamical) state of seawater. For measuring the conductivity of electrolytic solutions, there are, in principle, two groups of sensors (As it has been seen in the previous chapter 1): 1) classical conductivity cells containing two or more electrodes; 2) inductive conductivity sensors containing one or two transformers. In oceanographic work this type of sensors has found broad application [1]. In this experimental project the second sensor will be used and, for this reason, it is better to illustrate in detail the exact theory of inductive conductivity sensors derivated by Klaus Striggow and Reinhard Dankert in the 1984 [7]. 2.1 The Exact Theory of Inductive Conductivity Sensors As is well known, inductive sensors have the advantage that there are no electrodes, which suffer from polarization and fouling thereby preventing long-term stability [8]. But, there is a new problem caused by the variability of the permeability of the transformer core(s) due to its temperature and pressure dependence. During in situ measurements, temperature and pressure can often quickly vary over the intervals -2°C ≤T ≤ 30°C and 0 ≤ p≤ 108 Pa. As is shown in Figure 2.1, the permeability of transformer-core materials is a nonlinear function of T and p which, additionally, is influenced by relaxation and hysteresis. 24 CHAPTER 2 THE INDUCTIVE CONDUCTIVITY SENSOR (a) (b) Figure 2.1 - Dependence of the normalized permeability u/u(0,0) of transformer core materials on: (a) temperature T and (b) pressure P. u(0, 0) is the initial value of the permeability in a temperature pressure cycle. Pay attention to nonlinearity, relaxation, and hysteresis. (Muniperm is a metallic material, Manifer 110 and 150 are ceramic core materials produced by VEB Keramische Werke HermsdorfiThiir. Magnetic materials of other producers may not be expected to have less complicated properties.) In this project the pressure dependence of the permeability is not important because the remote node of the sensors is dislocated only up the river and not at down level. For the temperature there aren’t problem again with the permeability effect because the temperature of the water in the Tagus estuary is surely between the intervals -2°C ≤ T ≤ 30°C The exact theory of inductive conductivity sensors for oceanographic, that now it is being described, will be based on two commonly used types of inductive conductivity sensors: • single transformer; • double transformer. 2.1.1 The Single Transformer The simplest form of the inductive conductivity sensor for a liquid is a transformer, the secondary coil of which is formed by the surrounding liquid, here the seawater (see Figure 2.2). The primary current is then the sensor output signal. 25 CHAPTER 2 THE INDUCTIVE CONDUCTIVITY SENSOR Figure 2.2 - The single transformer as conductivity sensor: construction. (G: case, K: ringshaped core of the transformer, l: primary coil of the transformer, M: seawater loop (= secondary coil)). The relationship who exists between the resistance Rw, of the seawater loop and the sensor output I1 is: ⎛ 1 1 ⎞ I1 = ⎜ 2 + ⎟ U1 ⎝ n1 Rw jω L11 ⎠ (2.1) where: n1 is the number of windings; L11 the inductance of the (primary) coil; j= −1 , ω = 2πf, and f the frequency. The circuit of the Figure 2.2 is show in Figure 2.3 (a). Equation (2.1) directly leads to the equivalent circuit (see Figure 2.3(b)) of this type of sensor. (a) (b) Figure 2.3 – (a) circuit, (b) equivalent circuit. 26 CHAPTER 2 THE INDUCTIVE CONDUCTIVITY SENSOR Furthermore, it makes evident that the primary current I1 consists of two components: - the real or active component Ilact = [1/(n12Rw)]Ul being in phase with the primary voltage Ul, - and the imaginary component Ilimg = [(l/(jωLl1]U1 being in quadrature to the primary voltage. Obviously Ilact is a function of Rw alone, and not of the inductance L11. Therefore the real component of the primary current is a measure of the conductivity, independent of permeability of the core! Although this configuration is very simple it has not been applied to oceanographic conductivity sensors. There are several methods available to determine the active component Ilact of the primary current I1: 1) The peak value Iˆ1 , of the primary current Il, as well as its phase shift φ against the primary voltage Ul are measured (Figure 2.4). Figure 2.4 – Primary current if the primary voltage is sinusoidal Then the peak value Iˆ1act of the active component can be calculated by Iˆ1act = Iˆ1 cos ϕ 2) The peak value Iˆ1act of the active component is measured directly by sampling the primary current exactly at that moment when the primary voltage passes its maximum (Figure 2.4). 27 CHAPTER 2 THE INDUCTIVE CONDUCTIVITY SENSOR 3) The peak or mean value oft he active component of the primary current is measured by means of a wattmeter. 4) The sensor is shunted with a capacitance C. Based on the equivalent circuit of the sensor (Figure 2.3b) and ( 2.l ) , the total input current is ⎛ 1 ⎞ 1 + jωC ⎟ U1 I1total = ⎜ 2 + ⎝ n1 Rw jω L11 ⎠ (2.2) By choosing C so that ωC = 1/(ωL11), the reactive or imaginary component vanishes, and Iltotal becomes an exact measure for Rw. 5) The sensor is designed in such a manner that the condition ωL11 >> n12 Rw is satisfied. Then, according to (2.1) , the imaginary component becomes sufficiently small and the primary current becomes an approximative measure of Rw. 2.1.2 The Double Transformer The double transformer is used for measuring the conductivity of liquids and is widely applied to oceanographic instrumentation. The double transformer consists of two transformers where a water loop forms both the secondary coil of the first transformer (“driver transformer”) and the primary coil of the secondary transformer (“pickup transformer”) (see Figure 2.5(a) and (b)). (a) 28 THE INDUCTIVE CONDUCTIVITY SENSOR CHAPTER 2 (b) Figure 2.5 – The double transformer as conductivity sensor: (a) construction and (b) circuit. (K1, K2: ringshaped cores oft he first and second transformer, 1, 4: primary coil of the first and secondary coil of the second transformer, M: seawater loop ( = secondary coil of the first as well as primary coil of the second transformer)). It is important to arrange the two transformers in such a manner that the only coupling between them is by the common water loop. The voltage or current of the second coil of the pickup transformer is considered as the sensor output signal. The relationship between Rw and U4 is: U4 = n4 n1 1 U1 ⎛ 1 1 ⎞ 2 1 + n4 Rw ⎜ + ⎟ ⎝ RA jω L44 ⎠ (2.3) Up to now, oceanographic applications have taken advantage of three special cases involving (2.3). 1) The short-circuit current I4,K is a measure of Rw which is independent of the inductance L44, i.e., the permeability. Indeed, from (2.3) it follows that: I 4,k = lim (U 4 / RA ) = RA → 0 29 1 U1 n1n4 Rw (2.4) CHAPTER 2 THE INDUCTIVE CONDUCTIVITY SENSOR 2) Used a very small terminating resistor RA satisfying the condition RA << ωL44. In this special case, according to (2.3), U4 becomes nearly independent of L44. 3) Shunted the terminating resistor RA with a capacitor C in their instrument. Then in (2.3) the term 1/RA must be substituted by ((l/RA) + jωC). If C satisfies the condition ωC ≈ l/(ωL44), the imaginary terms within the bracket cancel, and U4 becomes (nearly) independent of L44. The (2.3) reveals further possibilities for eliminating the unwanted effect of shifting permeability. After transformation to the equivalent form U1 = n1 ⎛ n4 2 Rw jn4 2 Rw ⎞ − ⎜1 + ⎟U n4 ⎝ RA ω L44 ⎠ 4 (2.5) (2.3) allows the following interpretation. U1 can be decomposed into two components, the first of which n1 ⎛ n4 2 Rw ⎞ ⎜1 + ⎟U 4 n4 ⎝ RA ⎠ is in phase with U4 and independent of permeability, whereas the second ⎛ jn1n4 Rw ⎞ ⎜− ⎟U 4 ⎝ ω L44 ⎠ has a phase lag of 90” relative to U4, and depends on L44. This directly leads to the following methods. 4) U1 and U4 are sampled when the latter passes its maximum. Because at this moment the quadrature component ( - j … U4) crosses zero, it follows from (2.5) that U1* = n1 ⎛ n4 2 Rw ⎞ ˆ ⎜1 + ⎟U 4 n4 ⎝ RA ⎠ (2.6) where U1* denotes the measured momentary value of U1. This equation allows the determination of Rw independent of perrneability. 30 CHAPTER 2 THE INDUCTIVE CONDUCTIVITY SENSOR 5) The peak values of both U1, and U4 are sampled as well as the phase angle φ between them. After having calculated U1* = Uˆ1 cos φ , Rw can be determined as described under 2.4). 6) U1, and U4 are brought to an averaging multiplier. Then according to (2.5) we find 2 U1 = n1 ⎛ n4 2 Rw ⎞ ⎜1 + ⎟ U1U 4 n4 ⎝ RA ⎠ (2.7) Where the bar denotes time averaging. This equation again is independent of permeability. 2.2 The inductive conductivity cell for water salinity monitoring In these paragraphes an inductive sensor constructed as a double transformer is describe, to be utilized to measure the water salinity in the sea and estuaries. This inductive sensor has been developed at the Instituto de Telecomunicacoes of Lisbon [9]. 2.2.1 Sensor design The sensor structure is shown in Figure 2.6. Two toroidal cores of amorphous iron are mounted together as shown in Figure 2.6. Each core is provided with one winding of 20 turns. This assemble is immersed in the aqueous solution. A plastic container is used to delimit the lines of current inside the water, preventing the influence of strange objects on the measuring process. Therefore all the current in the water is enclosed by the plastic container. However, the container is provided with some apertures to let the water flow through the cell. The expected lines of current are depicted in the Figure 2.7. 31 CHAPTER 2 THE INDUCTIVE CONDUCTIVITY SENSOR Figure 2.6 - Cell structure: two cores with one winding each inside a plastic container. 42 13 40 136 22 Figure 2.7 - Lines of current embracing the two toroids inside the plastic container. The dimensions are in millimeters. The cell will work in an alternate sinusoidal regime. However, the resistance of the water path may be calculated assuming stationary fields, if the depth of penetration δ in the water is much greater than the cell dimensions for the maximum frequency of operation. Considering the maximum frequency as f max = 50 kHz and σ max = 5 S/m we obtain using (2.8), a value for the depth of penetration of the order of one meter. This will guarantee that the depth of penetration of the electromagnetic field in the salty water will always be greater than the dimensions of the sensor, for the entire range of the conductivities to be measured. δ min = 2 ωmax μ0σ max (2.8) 2.2.2 Sensor modelling The finite element method was used to estimate the configuration of the electric field induced inside the cell. As shown in the previous section the current field can be 32 CHAPTER 2 THE INDUCTIVE CONDUCTIVITY SENSOR determined as in the dc-regime. Equipotentials and lines of current were determined using this method. The lines of current are shown in the Figure 2.8. These results allow the determination of the water resistance and of the cell constant. This modeling shows that the resistance RW of the water path may be written in the form, RW = KC σ (2.9) where KC is the cell constant, which only depends on the geometric shape. In our case and for the linear dimensions presented on the Figure 2.7 the value KC = 110 m-1 was obtained. Figure 2.8 - Current lines obtained using the finite element method. The electric circuit represented in Figure 2.9 is useful to preview the electric behavior of the presented sensor. However in this scheme the dispersion of the magnetic field lines and the resistance of the wire windings are neglected. The effect of parasitic capacitances is not taken into account. Figure 2.9 - Sensor schematic circuit: RW represents the resistance of the water circuit. The circuit represented in Figure 2.9 has an equivalent as represented in Figure 2.10. The first transformer is represented by the electric circuit as seen from the primary (the winding of 20 turns) and the second transformer as seen from the secondary (20 turns output). In this equivalent circuit Z represents the impedance of the 20 coils around one toroidal core. It was verified by measurement that, at the frequency of 50 kHz, the impedance Z presented an important real part with an angle of losses greater than π / 4 . However, the frequency of 50 kHz was chosen because the sensibility increases with frequency. It was 33 CHAPTER 2 THE INDUCTIVE CONDUCTIVITY SENSOR also verified that the impedance Z did not present important variations for input amplitude voltage variations between 5 and 10 volt. Figure 2.10 - Equivalent circuit of the double transformer sensor. With this model it was possible to preview the behavior of the sensor when it was driven by a constant voltage source or when it was driven by a constant current source. For a voltage of imposed constant amplitude applied to the input transformer the expected output voltage phasor will be U out = U in Z Z + n 2 RW (2.10) A close examination of the expression (2.10) shows that the expected sensitivity of the output voltage to the water resistance RW varies largely in the range of measurement: dU out − Zn 2U in = dRW ( Z + n 2 RW )2 (2.11) Being the range of the conductivity measurement (100 mS/m < σ < 5 S/m) , and taking the equation (2.9) into account, the corresponding values of the water resistance RW will be in U =1 V the interval (1.1 kΩ > RW > 22 Ω) . For Z = (3.2∠37º ) kΩ and in , the sensitivity given by (2.11) will be in the interval 6, 54 ×10−6 < dU out < 9, 64 ×10−3 V/Ω dRW (2.12) The sensitivity of the output voltage to the conductivity σ , also for unitary input voltage, will be given by dU out dU out dRW = dσ dRW d σ which corresponds to the interval 34 (2.13) CHAPTER 2 THE INDUCTIVE CONDUCTIVITY SENSOR 72 > dU out > 42 mV/(S/m) dσ (2.14) These results show that the expected absolute errors inherent to the sensor are of the same order of magnitude, for low or high conductivities, but quite different in relative value. Therefore a special attention must be taken when projecting the electronic circuitry associated to the detection of the sensor output voltage. The sensor is driven by a sinusoidal oscillator working at f=50 kHz and rms output voltage of Uout=10 V. The components in phase and in quadrature of the sensor output voltage were measured separately. For a circuit with the topology of that shown in Figure 2.10, and for the values of Z and U out referred above, the output sensor voltage components will vary with RW as shown in the Figure 2.11. 1,2 Output Voltages (V) 1 0,8 0,6 0,4 0,2 0 0 100 200 300 400 500 600 700 800 900 1000 Water Resistance (Ω) Figure 2.11 - Cell output voltage. The upper curve is the component in phase and the lower curve the component π/2 out of phase with the sensor input. 2.2.3 Experimental characterization The cell was characterized in a bath of salty water by using an automated set-up previously developed. The cells were tested varying the frequency and the temperature, in baths of different salinities. Some of the obtained results are presented in Figure 2.12. These results show the dependence of the trans-impedance on the frequency, and were used to select the final frequency of operation for the prototype. 35 CHAPTER 2 THE INDUCTIVE CONDUCTIVITY SENSOR Transimpedance module for different temperatures 8 |Z21| (Ω) 6 20.0 °C 22.0 °C 24.0 °C 26.0 °C 28.0 °C 30.0 °C 4 2 0 0 5000 10000 15000 Frequency (Hz) 20000 25000 30000 Transimpedance phase for different temperatures 180 20.0 °C 22.0 °C 24.0 °C 26.0 °C 28.0 °C 30.0 °C Phase (º) 160 140 120 100 80 0 5000 10000 15000 Frequency (Hz) 20000 25000 30000 Figure 2.12 - Cell transimpedance as a function of frequency and temperature. The measurements correspond to a solution with conductivity of 43 mS/m at 20.0 ºC. Figure 2.12 shows clearly that the sensitivity increases with the frequency. These measurements were carried out in a bath with conductivity lower than the minimum conductivity of the measurement range. For this low conductivity value it was possible to separate the curves measured for different temperatures, and confirm the theoretical law of variation with the temperature. 36 Chapter 3 General Description of the Wireless Conductivity Sensing for Water Salinity Monitoring In this chapter the general characteristics of the proposed Conductivity Sensing Network Based On Wireless Transmission will be described with particular attention to the architecture and to the Oscillator, Microcontrollers and the RF module necessary for the main functionalities of the Remote Water Quality Monotoring System. 3.1 General architecture of Wireless Conductivity Sensing 3.1.1 Hardware architecture The Conductivity Sensing Network Based On Wireless Transmission is built as a master/slave architecture. The remote distributed measuring system includes a node called primary acquisition and processing units (PAPs). Each PAP contains the hardware inductive sensor interface, the inductive sensor, the temperature sensor, the processing unit and the RF module [10]. Communication between the PAPs and the central control and processing unit (CCP) is based on a RF transmission FSK modulation at 400 MHz or 900 MHz. Thus, the remote node that includes the microcontroller with port USART-RS232 and the RF module can be directly connected to the CCP in order to transmit the numerical values of water quality parameters from the zones to monitor. In the following two subsections, two network and communication architectures are presented: a RF – CCP, which was initially selected for building the first prototype illustrated in this work of thesis, and a RF – GSM/GPRS which will be developed in future works. 37 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING a) RF wireless transmission architecture The RF wireless communication is built as a master/slave architecture using the Star network topology. It is shown in Figure 3.1. PAP2 unit PAP3 unit Central Control and processing Unit - CCP Master node Primary Acquisition and Processing unit – PAP1 unit PAP4 unit Slave node Connection RF PAPn unit Figure 3.1 - Network Topology The wireless connection is based on a direct connection CCP-PAP unit node; all nodes are directly connected with the CCP. Each node is identified by a node address which identifies a node in the network in an univocal way. The type of transmission and receiving with RS232 is serial asynchronous half-duplex, where a byte is the single unit of transmission with the adding of the start bit and stop bit; the first bit transmitted is LSB, Least Significative Bit and the velocity of transmission can arrive at a bound rate of 38400. In Figure 3.2 is shown the basic idea of the project of the water quality system based on the RF wireless transmission architecture. 38 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING CCP unit RS232 Master RF Transceiver Directly connection Range 250 mt RF Transceiver PAP1 unit RF Transceiver PAP3 unit WQ sensors Water under test RF Transceiver C T WQ sensors PAP2 unit Slave Slave C T WQ sensors C T Slave Figure 3.2 – basic idea of the project The block diagram of the single PAP and the CCP implemented in the first prototype are shown in Figure 3.3. The node includes the sensor units, the conditioning circuit and a microprocessor unit, that establishes the interface between the sensors conditioning circuit and the transmission unit. Oscillator Inductive Sensor Sensor Analog to Digital Conversion Microprocessor Detection (a) 39 Low Power RF Transciever CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING Low Power RF Transciever RS232 Central PC Server (b) Figure 3.3 – General architecture of the first prototype (a) PAP unit, (b) CCP The work to be done is part of a project concerning the monitoring of the water quality in the Tagus river. Within the project, parameters like temperature, pH, conductivity, dissolved oxygen and turbidity are to be accessed in-situ. b) RF transceiver – GPS/GPRS Hybrid Architecture In order to reduce costs, to be able to increase the distance between the CCP and the monitored area, a hybrid architecture based on a RF transceiver and on GPS/GPRS modems will be designed and implemented. In Figure 3.4 the updated network topology is shown. CCP PAP2 unit PAP2 unit PAP3 unit GPRS PAP3 unit PAP1 unit GPRS PAP4 unit PAP1 unit PAPn unit PAP4 unit PAPn unit Figure 3.4 – Updated network topology 40 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING In Figure 3.5 is shown the updated basic idea of the project of the water quality system based on the RF - GPS/GPRS hybrid architecture. CCP unit RS232 GPRS modem RF Transciever PAP1 unit RF transciever RS232 GPRS modem Access Point WQ sensors Water under test C T RF Transciever RF Transciever PAP3 unit PAP2 unit WQ sensors WQ sensors C C T T Figure 3.5 – Updated of the basic idea of the project The theory of the most important components used in this project will be described in the next paragraph, such as the oscillator, the microcontrollers and the RF module in order to develop the main functionalities of the Remote Water Quality Monitoring System. 41 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING 3.2 General Architecture of Oscillator Oscillators are circuits that produce specific, periodic waveforms such as square, triangular, sawtooth, and sinusoidal. They generally use some form of active device, lamp, or crystal, surrounded by passive devices such as resistors, capacitors, and inductors, to generate the output. Oscillators are useful for generating uniform signals that are used as a reference in such applications as audio, function generators, digital systems, and communication systems. There are two main classes of oscillator: sinusoidal and relaxation. Sinusoidal oscillators consist of amplifiers with external components RC or LC circuits that have adjustable oscillation frequencies (the frequency and amplitude of oscillation are set by the arrangement of passive and active components around a central op amp), or crystals that have a fixed oscillation frequency. The focus here is on sine and cosine wave oscillators, created using operational amplifiers op amps. Relaxation oscillators generate triangular, sawtooth, square, pulse, or exponential waveforms, and they are not discussed here. Sine wave oscillators are used as references or test waveforms by many circuits. A pure sine wave has only a single or fundamental frequency - ideally no harmonics are present. Thus, a sine wave may be the input to a device or circuit, with the output harmonics measured to determine the amount of distortion. The waveforms in relaxation oscillators are generated from sine waves that are summed to provide a specified shape [11]. In this project the sine-cosine wave oscillator (the exactly name is the Quadrature oscillator) is used to drive the inductive sensor described in character 2 and to extract the component in phase and quadrature in output of the sensor inductive itself. Op-amp oscillators are restricted to the lower end of the frequency spectrum, because opamps do not have the required bandwidth to achieve low phase shift at high frequencies. Voltage-feedback op amps are limited to a low kHz range because their dominant, openloop pole may be as low as 10 Hz. The new current-feedback op amps have a much wider 42 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING bandwidth, but they are very hard to use in oscillator circuits because they are sensitive to feedback capacitance. Crystal oscillators are used in high-frequency applications up to the hundreds of MHz range. In this project the crystal oscillators will be used to give the clock frequency of the PIC (see chapter 5). 3.2.1 Requirements for Oscillation The canonical, or simplest, form of a negative feedback system is used to demonstrate the requirements for oscillation to occur. Figure 3.6 shows the block diagram for this system in which VIN is the input voltage, VOUT is the output voltage from the amplifier gain block (A), and β is the signal, called the feedback factor, that is fed back to the summing junction. E represents the error term that is equal to the summation of the feedback factor and the input voltage. Figure 3.6 - Canonical Form of a Feedback System With Positive or Negative Feedback The corresponding classic expression for a feedback system is derived as follows. Equation 3.1 is the defining equation for the output voltage; equation 3.2 is the corresponding error: VOUT = E × A (3.1) E = VIN + β VOUT (3.2) Eliminating the error term, E, from these equations gives VOUT = VIN − β VOUT A and collecting the terms in VOUT yields 43 (3.3) CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING ⎛1 ⎞ VIN = VOUT ⎜ + β ⎟ ⎝A ⎠ (3.4) Rearrangement of the terms produces equation 5, the classical form of feedback expression: VOUT A = VIN 1 + Aβ (3.5) Oscillators do not require an externally-applied input signal; instead, they use some fraction of the output signal created by the feedback network as the input signal. Oscillation results when the feedback system is not able to find a stable steady-state because its transfer function can not be satisfied. The system goes unstable when the denominator in equation 3.5 becomes zero, i.e., when 1 + A β = 0, or A β = –1 The key to designing an oscillator is ensuring that A β = –1. This is called the Barkhausen criterion. Satisfying this criterion requires that the magnitude of the loop gain is unity with a corresponding phase shift of 180º as indicated by the minus sign. An equivalent expression using the symbology of complex algebra is Aβ = 1 ∠ − 180° for a negative feedback system. For a positive feedback system, the expression is Aβ = 1 ∠0° and the sign of the A β term is negative in equation 3.5. As the phase shift approaches 180º and |A β| → 1, the output voltage of the now-unstable system tends to infinity but, of course, is limited to finite values by an energy-limited power supply. When the output voltage approaches either power rail, the active devices in the amplifiers change gain. This causes the value of A to change and forces Aβ away from the singularity; thus the trajectory towards an infinite voltage slows and eventually halts. At this stage, one of three things can occur: (i) Nonlinearity in saturation or cutoff causes the system to become stable and lock up at the current power rail. 44 CHAPTER 3 (ii) GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING The initial change causes the system to saturate (or cutoff) and stay that way for a long time before it becomes linear and heads for the opposite power rail. (iii) The system stays linear and reverses direction, heading for the opposite power rail. The second alternative produces highly distorted oscillations (usually quasi-square waves), the resulting oscillators being called relaxation oscillators. The third produces a sine-wave oscillator. 3.2.2 Phase Shift in the Oscillator The 180º phase shift in the equation Aβ = 1 ∠ − 180° is introduced by active and passive components. Like any well-designed feedback circuit, oscillators are made dependent on passive-component phase shift because it is accurate and almost drift-free. The phase shift contributed by active components is minimized because it varies with temperature, has a wide initial tolerance, and is device dependent. Amplifiers are selected so that they contribute little or no phase shift at the oscillation frequency. These constraints limit the op-amp oscillator to relatively low frequencies. A single-pole RL or RC circuit contributes up to 90° phase shift per pole, and because 180º of phase shift is required for oscillation, at least two poles must be used in the oscillator design. An LC circuit has two poles, thus it contributes up to 180º phase shift per pole pair. But LC and LR oscillators are not considered here because low frequency inductors are expensive, heavy, bulky, and highly nonideal. LC oscillators are designed in high frequency applications, beyond the frequency range of voltage feedback op amps, where the inductor size, weight, and cost are less significant. Multiple RC sections are used in low frequency oscillator design in lieu of inductors. Phase shift determines the oscillation frequency because the circuit oscillates at whatever frequency accumulates a 180° phase shift. The sensitivity of phase to frequency, dφ/dω, determines the frequency stability. When buffered RC sections (an op amp buffer provides high input and low output impedance) are cascaded, the phase shift multiplies by the number of sections, n (see Figure 3.7). 45 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING Figure 3.7 - Phase Plot of RC Sections In the region where the phase shift is 180°, the frequency of oscillation is very sensitive to the phase shift. Thus, a tight frequency specification requires that the phase shift, dφ, be kept within exceedingly narrow limits for there to be only small variations in frequency, dω, at 180°. Figure 3.7 demonstrates that, although two cascaded RC sections eventually provide 180° phase shift, the value of dφ/dω at the oscillator frequency is unacceptably small. Thus, oscillators made with two cascaded RC sections have poor frequency stability. Three equal cascaded RC filter sections have a much higher dφ/dω (see Figure 3.7), and the resulting oscillator has improved frequency stability. Adding a fourth RC section produces an oscillator with an excellent dφ/dω; thus, this is the most stable RC oscillator configuration. Four sections are the maximum number used because op amps come in quad packages, and the four-section oscillator yields four sine waves 45° phase shifted relative to each other. This oscillator can be used to obtain sine/cosine or quadrature sine waves. Crystal or ceramic resonators make the most stable oscillators because resonators have an extremely high dφ/dω as a result of their nonlinear properties. Resonators are used for high-frequency oscillators, but low-frequency oscillators do not use resonators because of size, weight, and cost restrictions. Op amps are not generally used with crystal or ceramic resonator oscillators because op amps have low bandwidth. Experience shows that rather than using a low-frequency resonator for low frequencies, it is more cost effective to build a high frequency crystal oscillator, count the output down, and then filter the output to obtain the low frequency [11]. 46 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING 3.2.3 Gain in the Oscillator The oscillator gain must be unity (Aβ = 1 ∠ − 180° ) at the oscillation frequency. Under normal conditions, the circuit becomes stable when the gain exceeds unity, and oscillations cease. However, when the gain exceeds unity with a phase shift of –180°, the nonlinearity of the active device reduces the gain to unity and the circuit oscillates. The nonlinearity becomes significant when the amplifier swings close to either power rail because cutoff or saturation reduces the active device (transistor) gain. The paradox is that worst-case design practice requires nominal gains exceeding unity for manufacturability, but excess gain causes increased distortion of the output sine wave. When the gain is too low, oscillations cease under worst case conditions, and when the gain is too high, the output wave form looks more like a square wave than a sine wave. Distortion is a direct result of excessive gain overdriving the amplifier; thus, gain must be carefully controlled in low-distortion oscillators. Phase-shift oscillators have distortion, but they achieve low-distortion output voltages because cascaded RC sections act as distortion filters. Also, buffered phase-shift oscillators have low distortion because the gain is controlled and distributed among the buffers. Most circuit configurations require an auxiliary circuit for gain adjustment when lowdistortion outputs are desired. Auxiliary circuits range from inserting a nonlinear component in the feedback loop, to automatic gain control (AGC) loops, to limiting by external components such as resistors and diodes. Consideration must also be given to the change in gain resulting from temperature variations and component tolerances, and the level of circuit complexity is determined based on the required stability of the gain. The more stable the gain, the better the purity of the sine wave output [11]. 3.2.4 Effect of the Active Element (Op Amp) on the Oscillator Until now, it has been assumed that the op amp has infinite bandwidth and the output is frequency independent. In reality, the op amp has many poles, but it has been compensated so that they are dominated by a single pole over the specified bandwidth. Thus, Aβ must now be considered frequency dependent via the op-amp gain term, A. Equation 3.6 shows this dependence, where a is the maximum open loop gain, ωa is the dominant pole 47 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING frequency, and ω is the frequency of the signal. Figure 3.8 depicts the frequency dependence of the op-amp gain and phase. The closed-loop gain, ACL = 1/β, does not contain any poles or zeros and is, therefore, constant with frequency to the point where it affects the op-amp open-loop gain at ω3dB. Here, the signal amplitude is attenuated by 3 dB and the phase shift introduced by the op amp is 45º. The amplitude and phase really begin to change one decade below this point, at 0.1 x ω3dB, and the phase continues to shift until it reaches 90º at 10 ω3dB, one decade beyond the 3-dB point. The gain continues to roll off at –20 dB/decade until other poles and zeros come into play. The higher the closed-loop gain, ACL, the earlier it intercepts the op-amp gain. A= a ω 1+ j ωa (3.6) The phase shift contributed by the op amp affects the performance of the oscillator circuit by lowering the oscillation frequency, and the reduction in ACL can make Aβ<1 and the oscillator then ceases to oscillate. Figure 3.8 - Op-Amp Frequency Response Most op amps are compensated and may have more than the 45º of phase shift at the ω3dB point. Therefore, the op amp should be chosen with a gain bandwidth at least one decade above the oscillation frequency, as shown by the shaded area of Figure 3.8. The Wien bridge requires a gain bandwidth greater than 43 ωOSC to maintain the gain and frequency within 10% of the ideal values [12]. 48 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING Care must be taken when using large feedback resistors because they interact with the input capacitance of the op amp to create poles with negative feedback, and both poles and zeros with positive feedback. Large resistor values can move these poles and zeros into the neighborhood of the oscillation frequency and affect the phase shift [13]. Final consideration is given to the op amp’s slew-rate limitation. The slew rate must be greater than 2πVPf0, where VP is the peak output voltage and f0 is the oscillation frequency; otherwise, distortion of the output signal results. 3.2.5 Analysis of Oscillator Operation (Circuit) Oscillators are created using various combinations of positive and negative feedback. Figure 3.9 (a) shows the basic negative feedback amplifier block diagram with a positive feedback loop added. When positive and negative feedback are used, the gain of the negative feedback path is combined into a single gain term (representing closed-loop gain). Figure 3.9 (a) reduces to Figure 3.9 (b), the positive feedback network is then represented by β = β2, and subsequent analysis is simplified. When negative feedback is used, the positive-feedback loop can be ignored because β2 is zero. (a) (b) Figure 3.9 - Block Diagram of an Oscillator: a) Positive and Negative Feedback Loops b) Simplified Diagram The general form of an op amp with positive and negative feedback is shown in Figure 3.10 (a). 49 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING The first step in analysis is to break the loop at some point without altering the gain of the circuit. The positive feedback loop is broken at the point marked with an X. A test signal (VTEST) is applied to the broken loop and the resulting output voltage (VOUT) is measured with the equivalent circuit shown in Figure 3.10 (b). (a) (b) Figure 3.10 - Amplifier With Positive and Negative Feedback: a) Original Circuit b) Loop Gain Calculation Equivalent Circuit First, V+ is calculated using equation 3.7; then it is treated as an input signal to a noninverting amplifier, resulting in equation 3.8. Substituting equation 3.7 for V+ in equation 3.8 gives the transfer function in equation 3.9. The actual circuit elements are then substituted for each impedance and the equation is simplified. These equations are valid when the op-amp open-loop gain is large and the oscillation frequency is less than 0.1 ω3dB. ⎛ Z3 ⎞ V+ = VTEST ⎜ ⎟ ⎝ Z3 + Z4 ⎠ (3.7) ⎛ Z + Z2 ⎞ VOUT = V+ ⎜ 1 ⎟ ⎝ Z1 ⎠ (3.8) VOUT ⎛ Z 3 ⎞ ⎛ Z1 + Z 2 ⎞ =⎜ ⎟⎜ ⎟ (3.9) VTEST ⎝ Z 3 + Z 4 ⎠ ⎝ Z1 ⎠ 50 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING Phase-shift oscillators generally use negative feedback, so the positive feedback factor (β2) becomes zero. Oscillator circuits such as the Wien bridge use both negative (β1) and positive (β2) feedback to achieve a constant state of oscillation. 3.2.6 Sine Wave Oscillator Circuits There are many types of sine wave oscillator circuits and variants - in an application, the choice depends on the frequency and the desired monotonicity of the output waveform. The focus of this section is on the more prominent oscillator circuit: Quadrature. 3.2.6.1 Quadrature Oscillator The quadrature oscillator shown in Figure 3.11 is another type of phase-shift oscillator, but the three RC sections are configured so each section contributes 90º of phase shift. This provides both sine and cosine waveform outputs (the outputs are quadrature, or 90º apart), which is a distinct advantage over other phase-shift oscillators. The idea of the quadrature oscillator is to use the fact that the double integral of a sine wave is a negative sine wave of the same frequency and phase, in other words, the original sine wave 180º phase shifted. The phase of the second integrator is then inverted and applied as positive feedback to induce oscillation [17]. The loop gain is calculated from equation 3.10. When R1C1 = R2C2 = R3C3, equation 3.10 reduces to equation 3.11. When ω = 1/RC, equation 3.14 reduces to ∠ − 180° , so oscillation occurs at ω = 2πf = 1/RC. The test circuit oscillated at 1.65 kHz rather than the calculated 1.59 kHz, as shown in Figure 3.12. This discrepancy is attributed to component variations. Both outputs have relatively high distortion that can be reduced with a gainstabilizing circuit. The sine output had 0.846% distortion and the cosine output had 0.46% distortion. Adjusting the gain can increase the amplitudes. The penalty is reduced bandwidth. ⎞ ⎛ 1 ⎞⎛ R3C3 s + 1 Aβ = A ⎜ ⎟⎟ ⎟ ⎜⎜ ⎝ R1C1s ⎠ ⎝ R3C3 s ( R2C2 s + 1) ⎠ 51 (3.10) CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING ⎛ 1 ⎞ Aβ = A ⎜ ⎟ ⎝ RCs ⎠ 2 (3.11) Figure 3.16 - Quadrature Oscillator Figure 3.12 - Output of the Circuit in Figure 3.11 52 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING 3.3 Microcontrollers Designer A MCU (Micro Controller Unit) is a programmable electronic device that is able to perform different functions in autonomously way. It is provided of CPU, RAM, Timer, a lot of input/output lines and devices to send and receive data. The principal difference between MCU and general microprocessor is that on the MCU all components are integrated on only one chip, while for the microprocessor the use of external devices is necessary. An embedded system is typically a design making use of the power of a small micro-controller, like the Microchip PICmicro® MCU or dsPIC® Digital Signal Controller (DSCs). The main difference between an embedded controller and a PC is that the embedded controller is dedicated to one specific task or set of tasks. A PC is designed to run many different types of programs and to connect to many different external devices. An embedded controller has a single program and, as a result, can be made cheaply to include just enough computing power and hardware to perform that dedicated task. A PC has a relatively expensive generalized central processing unit (CPU) at its heart with many other external devices (memory, disk drives, video controllers, network interface circuits, etc.). An embedded system has a low-cost microcontroller unit (MCU) for its intelligence, with many peripheral circuits on the same chip, and with relatively few external devices [18]. MCU are mainly used in the application with low power of calculation, but more speed of control. These devices are largely used in remote sensing, where it is possible to create a network of microcontrollers in order to form a centralized or decentralized system connecting different microcontrollers to other computers or mainframes to elaborate the information. MCU are built with CMOS technology that requires low energy for their power supply. The typical architecture of MCU can be subdivided into: • Harvard; • Von Neumann. 53 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING In Harvard Architecture there are two bus and memory: one for data and the other for instruction; while, in Von Neumann Architecture there is one bus and memory shared for data and instruction. Figure 3.13 - Harvard architecture vs Von Neumann architecture The advantage of Harvard Architecture is that the operation of fetch and execution can be done parallelly, reducing in this way the execution time. Besides, MCU can use two different types of instruction set: • CISC (Complex Instruction Set Computer); • RISC (Reduced Instruction Set Computer). The primary goal of CISC architecture is to complete a task in a few lines of assembly as possible. This is achieved by a building processor hardware that is capable of understanding and executing a series of operations. One of the primary advantages of this system is that the compiler has to do very little work to translate a high-level language statement into assembly. Because the length of the code is relatively short, very little RAM is required to store instruction. While, RISC processors only use simple instructions that can be executed within one clock cycle. At first, this may seem like a much less efficient way of completing the operation. Because there are more lines of code, more RAM is needed to store the assembly level instruction [19]. However the industries tendency is to use a RISC architecture for the following reasons: 1. easy planning; 2. reduced size of chip; 54 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING 3. low power use. Finally, in order to improve the performance, the best solution is the use of Harvard Architecture with pipelined RISC set instruction. 3.3.1 Microcontrollers choice The principal parameters for the choice of MCU are: 1. execution time of instruction; 2. availability of modules that are used for our application, for example A/D conversion module; 3. some tools that are available for both software and hardware uses, for example debbugger, simulator, possibility used C code and library. Figure 3.14 - Bit test and conditional branch Figure 3.15 - Loop control 55 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING Figure 3.16 - Synchronous transmission of 8 bit The previous Figures show the elaboration time for different cases, Loop Control, Bit Test, Conditional Jump, Synchronous Transmission of 8 bit, of different MCU. In all cases the MCU of Microchip have the best performance in comparison to the others, then according to the first case the MCU of Microchip is a good choice. For the second and the third case the Microchip supplies more software and hardware tools that can be used for the development of applications. At the end, since the MCU of Microchip are faster and there are many tools, of which more are free, the MCU of Microchip are the best choice for the aim of Remote Sensing [20]. 3.4 Intelligent RF module A generic RF system combine low power radio transmitters, receivers or transceivers with on-board microcontrollers to produce ‘intelligent’ RF modules that provide simple to use wireless data links. These links can be used for On/Off control tasks or for sending and receiving serial data, in standard formats, to and from host systems. There are four type of modules: transmitter, receiver, transceiver and frequency hopping. The ‘firmware’ within the microcontroller is optimised to suit the exact characteristics of the radio device and, there is no need to understand complex RF module parameters and all their implications. The task of encoding and decoding data in a suitable format for sending over a radio link is handled entirely within the device, as is error checking, that ensures the integrity of the messages. 56 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING Within the more sophisticated transceivers this firmware relieves the user of the complex mathematical task of programming synthesiser transmit or receive frequencies and also provides the complete management of the ‘frequency hopping’ versions of transceivers. In addition key parameters such as frequency of operation, data rate and power output can be programmed during product manufacture/assembly and prior to final test. This allows modules to be ‘tailored’ for specific applications or regional markets (e.g. Europe/USA) [22]. This paragraph describes the typical RF system configuration: “one way” and “two way”. 3.4.1 ‘One Way’ Easy-Radio for Transmitters & Receivers ‘One Way’ modules use FM transmitters and receivers in combination with on-board microcontrollers and a voltage regulator to provide simplex (one way) wireless data links. Figure 3.17 shows the block diagram for these modules. In addition to the usual supply (Vcc) and the 0 Volt (Ground) pins the transmitter has a Transmit Data (TXD) input and the receiver has a Data Out pin, a Received Signal Strength Indicator (RSSI) output and three configurable General Purpose Input/Output (GPIO) pins [23]. Figure 3.17 - Transmitter & Receiver Block Diagram 57 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING Application & Operation TS & RS Figure 3.18 shows a typical system block diagram comprising hosts (user’s application) connected to Transmitters and Receivers. Host (A) will be monitoring (collecting data) and Host (B) will be receiving and processing this data. Figure 3.18 - Typical System Block Diagram The Host (A) should provide the serial data input (up to a maximum 180 characters per packet) to the Easy-Radio transmitter. The data should be sent in ‘bursts’ therefore allowing adequate time for transmission and reception over the RF link. The receiver, upon reception and decoding of the RF transmission immediately sends serial data to the Host B. Data is sent and received in standard ‘RS232’ serial format (logic level only) and there is no restriction on the characters that may be sent. (HEX 00 – FF) A. Host (A) sends serial data to the Easy-Radio Transmitter (A). The data must be continuously streamed at the selected baud rate and it loads an internal transmit buffer until either it is full or a gap of two bytes is detected. B. After detecting either the ‘End of Data’ gap or the ‘Buffer Full’ condition the controller enables RF transmit and sends the data in the buffer using Manchester coding for efficient transmission across the RF link. Any Easy-Radio receivers within range that ‘hear’ the transmission will simultaneously decode the data and place it into their receive buffers. C. After checking the data for integrity, the Data within the receive buffer of EasyRadio Receiver (B) is then sent continuously to the host at the selected baud rate. 58 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING There is no ‘RF handshaking’ provided at either the transmitter or receiver. The user should therefore ensure that sufficient time is allowed for the completion of transmission and reception of data. Transmitter Host (A) must allow time for the ‘Over Air’ transmission and for the receiving Host (B) to unload (and process) the data before sending any more new data. The receiver Host (B) must always be ‘ready and waiting’ for data to arrive. It should be possible to use fast response ‘interrupts’ without any loss of data. With such a ‘one-way’ (simplex) system there is no confirmation of the satisfactory reception of the data and for added reliability it is recommended that the data be sent, perhaps, repetitively several times. For increased reliability the use of transceivers (which can acknowledge packet reception) is recommended. Easy-Radio services do not provide automatic acknowledgement (or re-tries) but these can be provided by the users application. Figure 3.19 - Serial Data 3.4.2 ‘Two Way’ for Transceivers Easy-Radio Transceivers are complete sub-systems that combine a high performance very low power RF transceiver, a microcontroller and a voltage regulator (Figure 3.20). The microcontroller programmes the functions of the RF transceiver and provides the interface to the host system via a serial input/output. It also contains programmable EEPROM memory that can hold configuration data for the various transceiver operating modes. A Received Signal Strength Indicator (RSSI) output can be optionally used to measure received signal levels. 59 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING Figure 3.20 - EasyRadio Transceiver Block Diagram The Serial Data Input and Serial Data Output operate at the standard 19,200 Baud and the two handshake lines provide optional flow control to and from the host. The Easy-Radio Transceiver can accept and transmit up to 180 bytes of data, which it buffers internally before transmitting in an efficient over-air code format. Application & Operation TRS Figure 3.21 shows a typical system block diagram comprising hosts (user’s application) connected to Easy-Radio Transceivers. The hosts (A & B) will be monitoring (collecting data) and/or controlling (sending data) to some real world application. Figure 3.21 - Typical System Block Diagram The hosts provide serial data input and output lines and two ‘handshaking’ lines that control the flow of data to and from the Easy-Radio Transceivers. The ‘Busy’ output line, when active, indicates that the transceiver is undertaking an internal task and is not ready 60 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING to receive serial data. The ‘Host Ready’ input is used to indicate that the host is ready to receive the data held in the buffer of the Easy-Radio Transceiver. The host should check before sending data that the ‘Busy’ line is not high, as this would indicate that the transceiver is either transmitting or receiving data over the radio link. It should also pull the ‘Host Ready’ line low and check that no data appears on the Serial Data Output line. Figure 3.22 provides a more detailed explanation of flow control. Figure 3.22 - Timing Diagram A. Host (A) sends serial data to the Easy-Radio Transceiver (A). Before doing so the host should check that the ‘Busy Output’ handshake line is low (Clear to Send data). The data must be continuously streamed at the selected baud rate and it fills an internal transmit buffer until either 180 bytes have been received or a gap of two bytes is detected. B. After detecting either the ‘End of Data’ gap or the ‘Buffer Full’ condition EasyRadio Transceiver (A) sets the ‘Busy’ output handshake line high. It then enables the RF transmit section of the transceiver and sends a 5mS preamble followed by the data in the buffer which is Manchester encoded at 19,200 Baud for efficient transmission across the RF link. C. Any Easy-Radio Transceivers within range that ‘hear’ the transmission will simultaneously lock onto the preamble, decode the data and place it into their receive buffers. D. The ‘Busy Output’ goes high during the decoding process and will remain high until the receive buffer is empty. The host should not send new data to the 61 CHAPTER 3 GENERAL DESCRIPTION OF WIRELESS CONDUCTIVITY SENSING FOR WATER SALINITY MONITORING transceiver if this line is high, should it attempt to do so the data will be ignored and therefore lost. E. Host (B) should indicate to Easy-Radio Transceiver (B) that it is ready to receive the data by setting the ‘Host Ready’ line low. When there is data in the buffer it will appear on the Serial Data Output. When the buffer is empty the Busy Output will go low. F. Data within the buffer then flows from the Easy-Radio Transceiver (B) to the host. The host can control the flow of data at any time by raising the Host Ready line to stop the data and lowering the line to continue the flow of data. After the host has received all the data (detected by either no more data or a minimum two byte gap in the data) it should then return the ‘Host Ready’ line high. 3.4.3 RSSI - Received Signal Strength Indicator The Receiver/Transceiver has a built in RSSI (Received Signal Strength Indicator) that provides an analogue output voltage that is inversely proportional to the RF energy present within the pass band of the receiver. It ranges from 0 Volt (maximum signal, –65dBm) to 1 Volt (minimum signal, -115dBm) and has a slope of approximately 50dB/Volt. This analogue output signal should only be connected to a high impedance load (>100k.s) and can be used to provide a measure of the signal strength and any interfering signals (noise) within band during the installation and operation of systems. Figure 3.32 - RSSI Output 62 Chapter 4 Hardware Inductive Sensor Interface In this chapter the project and construction of a first PCB (Printed Circuit Board) to drive an inductive conductivity sensor for water salinity monitoring will be presented. The sensor used is an inductive conductivity sensor double transformer developed and built by Instituto de Telecomunicações (it) in Lisboa and already described in the previous chapter 2. This sensor have two toroidal cores of amorphous iron mounted together. Each core is provided with one winding of 20 turns. It is important to build a circuit that drive the first toroidal core with an oscillator and measure the output voltage in the secondary toroidal core, as illustrated in Figure 4.1 [25]. Figure 4.1 - Electrodeless conductivity cell and instrumentation. The PCB has the following functions: 1) driving the inductive sensor by a sinusoidal oscillator. This oscillator has two outputs with exactly equal amplitudes but with a phase difference of π/2; 2) by using multipliers and convenient signal conditioning the amplitudes of the components in phase and of phase π/2 of the sensor output are obtained in the form of two dc-signals. Project and experimental results are presented. 63 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE 4.1 Electrical circuit of the Hardware Inductive Sensor Interface In Figure 4.2 a block diagram of the constructed hardware inductive sensor interface will be described for driving the sensor and to measure the output voltage, obtaining the components in phase and in quadrature with the input. For this purpose two integrated multipliers which incorporate low-pass filters necessary to extract the amplitudes of these components will be utilized. Power Supply +/-15 Volt Quadrature oscillator Multipliers DC component 2 COS DC component 1 Filters SIN V compensation 2 V compensation 1 Inductive Sensor Figure 4.2 - Block diagram of the circuitry to obtain the components in phase and π/2 out of phase with the sensor input voltage. The “schematic” of the PCB based on the block diagram of the Figure 4.2 is illustrated in Figure 4.3. The schematic was drawn with the program Altium Designer 6. Altium Designer provides an unified electronic product development environment, catering for all aspects of the electronic development process. For more details see the appendix C. The schematic is composed by the following parts and components: 64 CHAPTER 4 • • • • HARDWARE INDUCTIVE SENSOR INTERFACE Quadrature Oscillator; two Analog Multipliers AD633; low-pass filters; connectors. Figure 4.3 – Altium schematic of the Hardware Inductive Sensor Interface 65 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE 4.1.1 Quadrature Oscillator & operational amplifier TL082C In Figure 4.4 the electrical circuit of the Quadrature Oscillator is shown, which has two outputs, sine wave signal and cosine wave signal. The sine wave signal is used for driving the primary toroidal core of the inductive sensor and then together with the cosine wave signal is used to extract the components in phase and in quadrature from the output signal of the second toroidal core. This oscillator was projected to work at f = 50 kHz, because it is the better frequency for driving the sensor for the applications we need. [2-3] and the amplitude 12V pick to pick. Exactly the working frequency is 48,2 kHz because the analytic formula is f = 1 2πRC and, changing the value of resistor (R = 3.3 KΩ) and capacitor (C = 1nF), this value of frequency is obtain . Figure 4.3 - Electrical circuit of the Quadrature Oscillator 66 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE The Quadrature Oscillator uses an OP (operational amplifier) TL082C [26]. The TL082C is high speed J–FET input dual operational amplifiers incorporating well matched, high voltage J–FET and bipolar transistors in a monolithic integrated circuit. The devices feature high slew rates, low input bias and offset current, and low offset voltage temperature coefficient. The pin connections (top view) is shown in Figure 4.4 Figure 4.4 - The pin connection of the OP TL082C The features are: • Wide common-mode (up to Vcc+) and differential voltage range • Low input bias and offset current • Output short-circuit protection • High input impedance J–FET input stage • Internal frequency compensation • Latch up free operation • High slew rate : 16v/ms (typ) In Figure 4.5 the absolute maximum ratings of the TL082C is shown. In Figure 4.6 the maximum peak-to-peak output voltage versus frequency is shown. 67 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE Figure 4.5 - Absolute maximum ratings of the TL082C Figure 4.6 - Maximum peak-to-peak output voltage versus frequency It is also good practice to bypass the power supplies with quality capacitors. Low ESR (equivalent series resistance) 100 nF and 22 uF capacitors have been applied at the supplies of the operational amplifier to minimize transient disturbances and filter low frequency ripple. In Figure 4.7 the basic supply bypassing configuration used is illustrated. Figure 4.7 - Power Supply Bypassing 68 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE 4.1.2 Analog Multiplier - AD633 The AD633 is a low cost multiplier comprising a translinear core, a buried Zener reference, and a unity gain connected output amplifier with an accessible summing node. Figure 4.8 shows the functional block diagram. The differential X and Y inputs are converted to differential currents by voltage-to-current converters. The product of these currents is generated by the multiplying core. A buried Zener reference provides an overall scale factor of 10 V. The sum of (X × Y)/10 + Z is then applied to the output amplifier. The amplifier summing node Z allows the user to add two or more multiplier outputs, convert the output voltage to a current, and configure various analog computational functions [27]. Figure 4.8 - Functional Block Diagram (AD633JN Pinout Shown) Inspection of the block diagram shows the overall transfer function to be: W= ( X 1 − X 2 )(Y1 − Y2 ) + Z 10V (4.1) Figure 4.9 shows the basic connections for multiplication. The X and Y inputs will normally have their negative nodes grounded, but they are fully differential, and in many applications the grounded inputs may be reversed (to facilitate interfacing with signals of a particular polarity while achieving some desired output polarity) or both may be driven. Figure 4.9 - Basic Multiplier Connections In some instances, it may be desirable to use a scaling voltage other than 10V. The connections shown in Figure 4.10 increase the gain of the system by the ratio (R1 + 69 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE R2)/R1. This ratio is limited to 100 in practical applications. The summing input, S, may be used to add an additional signal to the output or it may be grounded. Figure 4.10 - Connections for Variable Scale Factor In the project of the hardware inductive sensor interface two Analog Multipliers AD633 are used to multiply the output of the inductive sensor (second toroidal core) by the sine wave signal (to extract the component in phase) and by the cosine wave signal (to extract the component in quadrature). The output of the sensor and the sine or cosine are therefore the two input X and Y of the multiplier. In the Figure 4.11 the electrical circuit of the two AD633 is shown; the resistance R1 in Figure 4.10 is now represented as R8 and R11 for the two multipliers and the value is 1KΩ; moreover R2 (Figure 4.10) is now represented in Figure 4.11 as three possible configurations of working: fixed resistance (R9 and R12), manual potentiometer (R14 and R15), or the possibility to control the value of scale by a digital potentiometer put in another PCB which controls the data by a microcontroller (this part is a future work). The value of the fixed resistance is different for the two multipliers, so that the first works better with the component in phase and the second works better with the component in quadrature. However before every multiplier a switch was put to decide if the multiplier works to extract the component in quadrature or in phase. All this is possible thanks to the two manual potentiometers (and in the future the digital potentiometers) which make the system flexible; 70 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE (a) (b) Figure 4.11 - Electrical circuit of the two AD633: (a) first multiplier and (b) second multiplier The features of the AD633 are: • 4-Quadrant Multiplication • Low Cost 8-Lead Package • Complete—No External Components Required 71 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE • Laser-Trimmed Accuracy and Stability • Total Error within 2% of FS • Differential High Impedance X and Y Inputs • High Impedance Unity-Gain Summing Input • Laser-Trimmed 10 V Scaling Reference The specification and the absolute maximum ratings of the AD633 are shown in Figure 4.12. The frequency Response is shown in Figure 4.13. Figure 4.12 - Absolute maximum ratings of the AD633 72 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE Figure 4.13 - Frequency Response of the AD633 4.1.3 Low-pass Filters In order to read the two DC components in output of the multipliers, two low-pass filters are necessary (one for every multiplier). The electrical circuits are shown in Figure 4.14; These filters RC have the values of R = 100KΩ (R10 and R13) and C = 100 nF (C8 and C11), so that the cutoff frequency is fc = 16Hz. (a) (b) Figure 4.14 - Electrical circuit of the two low-pass filters: (a) first (b) second The order of this two filter is the first. In fact in this application a simplex filter of the first order at the cutoff frequency fc = 16Hz is able to extract only the DC component signal as it will be seen by the analytic formula in output of the two multipliers: 73 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE - Component in phase Ai sin (ωt ) ⋅ Au sin (ωt + ϕ ) = Ai Au sin (ωt )sin (ωt + ϕ ) = Ai Au [cos(ϕ ) − cos(2ωt + ϕ )] = Ai Au cos(ϕ ) − Ai Au cos(2ωt + ϕ ) 2 2 2 DC term (4.2) AC term to filter - Component in quadrature Ai cos(ωt ) ⋅ Au sin (ωt + ϕ ) = Ai Au cos(ωt )sin (ωt + ϕ ) = Ai Au [sin (ϕ ) + sin (2ωt + ϕ )] = Ai Au sin (ϕ ) + Ai Au sin (2ωt + ϕ ) 2 2 2 DC term (4.3) AC term to filter In Figure 4.15 is shown frequency response of the filter. Figure 4.14 - Frequency response of the filter In the Figure it is possible to notice that at the frequency of 16kHz the attenuation is about -60dB. This dB will be chosen because the ADC resolution for the analog/digital conversion is a 10 bit and there is not a variation of signal down this value. The first harmonic is at 100 kHz so that it is not a problem. 74 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE The filter can remove also the frequency generated in the case the two sin o cosine waves don’t have exactly mean zero. In fact in this case the analytic formula is: [K1 + Ai sin (ωt )]⋅ [K 2 + Au sin (ωt + ϕ )] = = K1 K 2 + K1 Au sin (ωt + ϕ ) + K 2 Ai sin (ωt ) + Ai Au sin (ωt )sin (ωt + ϕ ) = = K1 K 2 + K1 Au sin (ωt + ϕ ) + K 2 Ai sin (ωt ) + (4.4) Ai Au AA cos(ϕ ) − i u cos(2ωt + ϕ ) 2 2 there is not only a double frequency at 100kHz but also the frequency at 50 kHz. However this is not a problem, because the filter cutoffs these frequencies. 4.1.4 Connectors The PCB uses 5 connector shown in Figure 4.15 Figure 4.15 - Connectors 75 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE The connectors P1, P2, P3, P4 and P5 have the following functions: • P1 is the connector for the power supply, where VCC is 15V and VEE is -15V; • P2 is the connector with the inductive sensor, where the pins 1 and 2 are connected with the primary toroidal core and the pin 3 an 4 are connected with the secondary toroidal core; • P3 is a connector to check if the quadrature oscillator works well. It is important that the sine and cosine wave signals have the same amplitude and frequency and that the phase difference between them is π/2; • P4 is the connector to change the scaling factor of the multipliers by the two digital multimeters. Vcomp1 and Vcomp2 are the analog outputs of the digital multimiters; • P5 is the connector to read the two DC components (phase and quadrature) in output of the inductive conductivity sensor. These two DC components will be processed by a microcontroller which, together with a temperature sensor, will extract the conductivity of the water. 4.2 Building PCB Hardware sensor interface After the schematic editor, the next step has been to convert the project in a PCB. In this case the program Altium Designer 6 has been used again, because it has this possibility. The components in the schematic have been converted in physical dimensions to put in the PCB and the ways of connection have been drawn with all the components. Only one layer (button layer) is used to make the building operation more easy. The PCB has been built in the IST (Instituto Superior Técnico) laboratories of Lisbon. In Figure 4.16 the PBC bottom layer is shown. 76 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE (a) (b) Figure 4.16 - Button layer of the PCB: (a) without ground, (b) with the ground for the final print In Figure 4.17 the PCB bottom printer without any electronic components is shown. Figure 4.17 - PCB bottom printer The PCB top printer with all electronic components is depicted in Figure 4.18. 77 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE Figure 4.18 - PCB top printer with all electronic components 4.3 Bill of materials 1° PCB In the table 4.1 there is a list of all the components and materials used to build the first PCB for the hardware inductive sensor interface. This list is composed of the name of the component, model and company, the name in the schematic, the value if is applicable, the quantity and the price in euro updated at September 2006 by Farnell Catalogue 2006. Picture Component /Model/Company Capacitor / MULTICOMP Polarized Capacitor (Axial) / MCGPR25V226M5X11/ MULTICOMP Designator Value C3, C5, C6, C7, C8, C9, C10, C11, C12, C14 C13, C15, C16, C17, C18, C19 1nF, 100pF 100nF 22uF Quantity Price € Total € 13 0,092 1,196 6 0,055 0,33 High Conductance Fast Diode / Diode 1N4148 / MULTICOMP D1, D2 2 0,012 0,024 Header, 3-Pin / CAMDEN ELECTRONICS P1, P3, P5 1 0,46 0,46 Header, 5-Pin / CAMDEN ELECTRONICS P2 1 0,83 0,83 78 CHAPTER 4 HARDWARE INDUCTIVE SENSOR INTERFACE Header, 2-Pin / CAMDEN ELECTRONICS P4 R1, R2, R3, R4, R5, R6, R7, R8, R9, R10, R11, Resistor / MULTICOMP R12, R13 Potentiometer R14, R15 TRIMMER, 22 TURN / T93YA / VISHAY SFERNICE 20KΩ 1 0,31 0,31 13 0,032 0,416 2 1,93 3,86 JFET-Input Operational Amplifier / TL082CP / TEXAS INSTRUMENTS U1 1 0,78 0,78 Low-Cost Analog Multiplier / AD633JN / ANALOG DEVICES U2, U3 2 11,00 22,00 3 0,22 0,66 4 0,05 0,20 MULTICOMP 2227MC-08-03-18 IC SOCKET, DIL 0.3" 8WAY Jumper Wire W1, W2, W3, W4 TOTALE 49 table 4.1 - Bill of materials 1° PCB 79 31.07 Chapter 5 Hardware Remote Node and Interface CCP Server In this chapter, the different modules to interface the microcontroller with the input/output line will be described by paying particular attention to the temperature sensor, digital potentiometer and the RF module devices. 5.1 Electrical Circuit of the Node Normally, each node is in state of receipt. This is the general architecture of the system, now let’s analyze the hardware architecture of the remote node. In Figure 5.1 the block diagram of node is illustrated. Power Supply +/- 15 Volt Voltage regulator Voltage regulator 5 Volt 3.3 Volt 4 MHz SDI CS2 oscillator CLK ANALOG INPUT V compensation 1 V compensation 2 Digital potentiometer CS1 PIC SDO SDI ADC DC component 1 0|1|0|0|1|1|1| 0 DIP Switch DC component 2 RF TRANSCEIVER Digital potentiometer ID Node Temperature sensor I/O Antenna Figure 5.1 - block diagram of a single node 80 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER The block diagram is composed of a battery +/- 15V and two voltage regulators of +5V and +3.3V, in order to have the power supply for all the components mounted on the PCB. It is composed of a PIC18F458 with a ADC 10-bit where are connected: three analog input (DC component1, DC component2 and temperature sensor), an oscillator at 4MHz, the two digital potentiometer for a future development, the RF transceiver ER900TRS (It is connected to PIC with the USART, Universal Serial Asynchronous Receiver Transmitter, at 19200 bit/sec with a packet of 8 bit). For the wireless transmission with the CCP, an DIP switch to store the address of the nodes is used. This reading is done at the reset of PIC an the use of DIP Switch allows an easy and quick change of the address of nodes. A monopole antenna with resonance frequency at 900 MHz has been used. The “schematic” of the PCB, based on the block diagram of the Figure 5.1, is shown in Figure 5.2. It has been drawn by the Altium Designer 6 program. The schematic is composed by the following parts and components: • Microcontroller PIC 18F458 with A/D converter • Temperature Sensor • Digital Potentiometer • DIP switch • RF module • Voltage regulator • Connectors 81 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER Figure 5.2 – Electrical circuit block diagram of a single node 82 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER 5.1.1 Microcontroller 18F458 Figure 5.3 - Image of PIC18F458 The Microcontroller that is used in the remote node is the 18F458. The principal characteristics of this PIC are [21]: • High-Performance RISC CPU: • 10-bit, up to 8-channel Analog-to-Digital Converter module (A/D) • 16-bit wide instructions, 8-bit wide data path • Linear program memory addressing up to 2 Mbytes • Linear data memory addressing to 4 Kbytes • DC – 40 MHz clock input • 4 MHz-10 MHz oscillator/clock input with PLL active • Priority levels for interrupts • 8 x 8 Single-Cycle Hardware Multiplier While, the peripheral features are: • Three external interrupt pins • Timer0 module: 8-bit/16-bit timer/counter with 8-bit programmable prescaler • Timer1 module: 16-bit timer/counter • Timer2 module: 8-bit timer/counter with 8-bit period register (time base for PWM) • Timer3 module: 16-bit timer/counter 83 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER • Secondary oscillator clock option – Timer1/Timer3 • Capture/Compare/PWM (CCP) modules; • Master Synchronous Serial Port (MSSP) • Universal Synchronous Asynchronous Receiver Transmitter with 9 – bit address detection. In Figure 5.4 the block diagram of the internal structure of the PIC18F458 is shown. Figure 5.4 - PIC18F458 block diagram There are three memory: Program Memory, Data Memory and EEPROM. The PIC18F258/458 devices have a 21-bit program counter that is capable of addressing a 2Mbyte program memory space. 84 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER Figure 5.5 - Program memory map and stack for PIC18F458 The data memory is partitioned into multiple banks which contain the General Purpose Registers and the Special Function Register, each bank, sixteen for 18F458, extends up to FFh (256 bytes). All data memory is implemented as static RAM. The Data EEPROM and FLASH program memory are readable and writable during normal operation over the entire VDD range. These operation take place on a single byte for Data EEPROM memory and a single word for program memory. A write operation causes an erase-then-write operation to take place on the specified byte or word. General purpose register file can be accessed either directly, or indirectly through the File Select Register, while the special function registers are registers used by the CPU ad peripheral modules for controlling the desired operation of the device and these are implemented as static RAM. The special function registers can be classified into two sets: core (CPU) and peripheral. The PIC18F458 is capable of addressing a continuous 8K word block of program memory. The CALL and GOTO instruction provide only 11 bits of address to allow branching within any 2K program memory page. Indirectly addressing is possible by using the INDF register. Any instruction using the INDF register actually accesses the register pointed to by the File Select Register, FSR. Some pins for these I/O ports are multiplexed with an alternate function for the peripheral features on the device. In general, when a peripheral is enabled, that pin may not be used as 85 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER a general purpose I/O pin. There are five bi-directional port: PORTA, PORTB, PORTC, PORTD, and PORTE; for setting these ports exists a corresponding data direction register: TRISA, TRISB, TRISC, TRISD and TRISE. If the bit ”x” of TRIS register is ”1”, then will make the corresponding PORT pin an input, while if the bit ”x” of TRIS register is ”0”, the will make the corresponding PORT pin as output. 5.1.1.1 Connections of the PIC18F458 The remote control is composed by a microcontroller PIC18F458, where all the devices are connected. The electrical circuit of PIC18F458 is shown in Figure 5.6. Figure 5.6 - Electrical circuit of PIC18F458 The PIC18F458 can be operated in one of eight oscillator modes, programmable by three configuration bits (FOSC2, FOSC1 and FOSC0) [21]. 1. 2. 3. 4. 5. 6. 7. 8. LP: Low-Power Crystal XT: Crystal/Resonator HS: High-Speed Crystal/Resonator HS4: High-Speed Crystal/Resonator with PLL enabled RC: External Resistor/Capacitor RCIO: External Resistor/Capacitor with I/O pin enabled EC: External Clock ECIO: External Clock with I/O pin enabled 86 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER In this case an easy crystal/resonator has been used. The values of the two capacitors (C14, C15) are identical to the ranges written on the datasheet for the 4MHz frequency. Higher capacitance increases the stability of the oscillator but also increases the start-up time. The reset of the PIC is a Power-on Reset (POR). The value of the R3 a C16 are used for give the time constant. The connections of the pins of the PIC are the following: Pins used Connections description 1 Power-on Reset (POR) 2,3,7,8,9,10 Analog Pins. They are used for the analog input to convert in digital. Exactly: AN0 is used to convert the first DC component in output to inductive sensor, AN1 to convert the second DC component in output to inductive sensor, AN4 to convert the analog output to the temperature sensor; AN5, AN6, AN7 are added analog inputs for future connections with other type sensors to control the water quality. 4,5 Pins to set the range of the A/D converter. Vref- is put to 0V and Vref+ is put to 5V. 11, 12, 31, 32 Power supply. 13, 14 Oscillator at 4 Mhz 18, 19, 20, 23 Pins used to connect the two digital potentiometers: 18–CLK, 19–CS2, 20– CS1, 23-SDI 25, 26 Pins used to connect the RF transceiver module: the pin RC6 is an input/output port pin, addressable USART asynchronous transmit or addressable USART synchronous clock; the pin RC7 is an input/output port pin, addressable USART asynchronous receive or addressable USART synchronous data. 33, 34, 35, PORTB used to give the ID of the remote node. It is connected the DIP36, 37, 38, Switch. 39, 40 87 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER 5.1.2 Temperature Sensor AD22103 In order to compensate the temperature, an AD22103 temperature sensor produced by Analog Devices company has been used. The AD22103 is a ratiometric temperature sensor IC whose output voltage is proportional to power supply voltage. The heart of the sensor is a proprietary temperature-dependent resistor, which is built into the IC. Figure 5.7 shows a simplified block diagram of the AD22103 [29]. Figure 5.7 - Simplified Block Diagram The temperature-dependent resistor, labeled RT, exhibits a change in resistance that is nearly linearly proportional to temperature. This resistor is excited with a current source that is proportional to power supply voltage. The resulting voltage across RT is therefore both supply voltage proportional and linearly varying with temperature. The remainder of the AD22103 consists of an op amp signal conditioning block that takes the voltage across RT and applies the proper gain and offset to achieve the following output voltage function: VOUT = VS [0.25V + (28.0mV / °C ) ⋅ TA ] 3.3V (5.1) This temperature sensor can be operated over the temperature range 0°C to +100°C, making it ideal for use in numerous 3.3 V applications. The formula 6.1 shows that the output voltage is proportional to the temperature times the supply voltage. The output swings from 0.25 V at 0°C to +3.05 V at +100°C using a single +3.3 V supply. 88 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER In Figure 5.8 are shown the PIN configuration and the PIN description of the AD22103. (a) (b) Figure 5.8 - (a) PIN configuration and (b) PIN description. Figure 5.9 graphically depicts the guaranteed limits of accuracy for the AD22103 and shows the performance of a typical part. As the output is very linear, the major sources of error are offset, i.e., error at room temperature, and span error, i.e., deviation from the theoretical 28.0 mV/°C. Demanding applications can achieve improved performance by calibrating these offset and gain errors so that only the residual nonlinearity remains as a source of error. Figure 5.9 - Typical AD22103 Performance The electrical schematic of the temperature sensor has been shown in Figure 5.10. It is composed of a connector with 3 PINS which connects the temperature sensor. 89 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER Figure 5.10 - Electrical schematic of the temperature sensor The pin 1 is used to drive the temperature sensor with a power supply of 3.3 volt. In order to have a voltage DC of 3.3 V, a block voltage regulator is used; it will be illustrated in the paragraph “Voltage regulator”. The pin 2 is connected to ground, as it is described in the AD22103 data sheet. The pin 3 is the output of the sensor of temperature. The relation between the output and the DC voltage in input to temperature sensor is described with the formula (5.1). In this case the Vs is 3.3V and the formula (5.1) becomes: VOUT = 0.25V + (28.0mV / °C ) ⋅ T A (5.2) In this case the range of the temperature sensor is [0°C – 100 °C] and according to the (5.2) and developing the passages (5.3), the output swings from 0.25 V at 0°C to +3.05 V at +100°C. (28.0mV / °C ) ⋅ TA = VOUT TA = VOUT − 0.25V 0.028V / °C 90 − 0.25V (6.3) CHAPTER 5 TA = HARDWARE REMOTE NODE AND INTERFACE CCP SERVER VOUT − 0.25V 0.028V / °C = 0°C ; TA = VOUT = 0.25V VOUT − 0.25V 0.028V / °C = VOUT =3.05V 2.8V = 100°C 0.028V / °C In this project a so big range of temperature has not been necessary, because the maximum temperature of the sea water recorded in the world has been 32 °C in the Red Sea, so that it has been decided to reduce the range of working between 0°C and 50 °C. The solution taken has been to use an operational amplifier KA741 by Fairchild [30] in the Non-Inverting Configuration with a gain G. In order to find the exactly value of G, which allows to obtain a 5V output voltage of the temperature sensor, when the water temperature is 50°C (in order to use all the Vref of the ADC), the following formula has been used: VOUT = [0.25V + (28.0mV / °C ) ⋅ T A ] ⋅ G (5.4) so G= VOUT 0.25V + (28.0mV / °C ) ⋅ T A TA =50° C VOUT =5V = 5V =3 0.25V + 1.4V Now changing the value of G, in the (5.4) it is possible to see that the range of the temperature sensor with the OP in input to A/D converter is [0°C – 50 °C] and the output swings from 0.75 V at 0°C to +5 V at +50°C VOUT = 0.25V ⋅ G + (28.0mV / °C ) ⋅ T A ⋅ G (28.0mV / °C ) ⋅ TA ⋅ G = VOUT TA = TA = − 0.25V ⋅ G VOUT 0.25V − (28.0mV / °C ) ⋅ G (28.0mV / °C ) VOUT 0.25V − = 0°C (28.0mV / °C ) ⋅ G (28.0mV / °C ) VOUT =0.75V G =3 91 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER TA = VOUT 0.25V − = 50°C (28.0mV / °C ) ⋅ G (28.0mV / °C ) VOUT =5V G =3 Now it is possible to compare the nominal resolution of the AD converter in case the system is without amplifier or with amplifier: - if the output of the sensor is without the operational amplifier and it has been put in a 10-bit A/D converter with a reference of 5V, there will be a least significant bit (LSB) size of 5V/1024 = 4.9mV. This corresponds to a nominal resolution of 0.175°C/LSB, in fact 3.05V – 0.25V = 2.8V and 2.8V divided by the range of 100°C is 28mV/°C, so we have 4.9mV/(28mV/°C) = 0.175°C/LSB. - if the output of the sensor is with the operational amplifier with gain G and it has been put in a 10-bit A/D converter with a reference of 5 V there will be always a least significant bit (LSB) size of 5V/1024 = 4.9mV, but now this corresponds to a nominal resolution of 0.06°C/LSB, in fact 5V – 0.75V = 4.25V and 4.25V divided by the range of 50°C is 85mV/°C, so we have 4.9mV/(85mV/°C) = 0.06°C/LSB. 5.1.3 Analog input and A/D conversion The three analog terminals (the two DC component in output to inductive sensor and the temperature sensor) of the A/D converter are protected by diodes (1N4148), as shown in Figure 5.11. Figure 5.11 - Protection Analog Pins 92 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER With this protection if the voltage of every analog input is more than 5 V ore less than 0 V, the diodes do not allow to put in the pin more than 5V ore less than 0V. The Analog-to-Digital (A/D) Converter module has eight inputs. This module has the ADCON0 and ADCON1 register definitions that are compatible with the PICmicro® midrange A/D module. The A/D allows conversion of an analog input signal to a corresponding 10-bit digital number. The A/D module has four registers. These registers are: • A/D Control Register 0 (ADCON0) - controls the operation of the A/D module (A/D Conversion Clock, Analog Channel Select, A/D Conversion Status and A/D On); • A/D Control Register 1 (ADCON1) - configures the functions of the port pins (A/D Result Format Select and A/D Port Configuration Control); • A/D Result High Register (ADRESH); • A/D Result Low Register (ADRESL) - The ADRESH and ADRESL registers contain the result of the A/D conversion. When the A/D conversion is complete, the result is loaded into the ADRESH/ADRESL registers, the GO/DONE bit (ADCON0<2>) is cleared and A/D Interrupt Flag bit, ADIF, is set. The analog reference voltage is software selectable to either the device’s positive and negative supply voltage (VDD and VSS) or the voltage level on the RA3/AN3/VREF+ pin and RA2/AN2/VREF- pin. The A/D converter has a unique feature of being able to operate while the device is in Sleep mode. To operate in Sleep, the A/D conversion clock must be derived from the A/D’s internal RC oscillator. The output of the sample and hold is the input into the converter which generates the result via successive approximation. 93 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER Each port pin associated with the A/D converter can be configured as an analog input (RA3 can also be a voltage reference) or as a digital I/O [21]. 5.1.4 Digital Potentiometer – AD7376 The AD7376 is one of the few high voltage, high performance digital potentiometers in the market at present. This device can be used as a programmable resistor or resistor divider. The AD7376 performs the same electronic adjustment function as mechanical potentiometers, variable resistors, and trimmers with enhanced resolution, solid-state reliability, and programmability. With digital rather than manual control, AD7376 provides layout flexibility and allows close-loop dynamic controllability [31]. The AD7376 features sleep-mode programmability in shutdown that can be used to program the preset before device activation, thus providing an alternative to costly EEPROM solutions. The AD7376 is available in 14-lead TSSOP and 16-lead wide body SOIC packages in 10 kΩ, 50 kΩ, and 100 kΩ options. All parts are guaranteed to operate over the -40°C to +85°C extended industrial temperature range. The functional block diagram of the AD7376 is shown in Figure 5.12. The PIN configuration is shown in Figure 5.13 and in the table 5.1 there are the PIN function descriptions Figure 5.12 – Functional block diagram 94 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER (a) (b) Figure 5.13 - (a) 14-Lead TSSOP Pin Configuration; (b) 16-Lead SOIC_W Pin Configuration table 5.1 - Pin Function Descriptions Programming the variable resistor The part operates in rheostat mode when only two terminals are used as a variable resistor. The unused terminal can be floating or tied to the W terminal as shown in Figure 5.14. Figure 5.14 - Rheostat Mode Configuration The nominal resistance between Terminals A and B, RAB, is available in 10 kΩ, 50 kΩ, and 100 kΩ with ±30% tolerance and has 128 tap points accessed by the wiper terminal. The 7bit data in the RDAC latch is decoded to select one of the 128 possible settings. Figure 5.15 shows a simplified RDAC structure. 95 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER Figure 5.15 - AD7376 Equivalent RDAC Circuit The general equation determining the digitally programmed output resistance between the W and the B terminals is RWB ( D) = D × R AB + RW 128 (5.5) where: D is the decimal equivalent of the binary code loaded in the 7-bit RDAC register from 0 to 127. RAB is the end-to-end resistance. RW is the wiper resistance contributed by the on resistance of the internal switch. Assuming that a 10 kΩ part is used, the wiper’s first connection starts at the B terminal for programming code of 0x00, where SWB is closed. The minimum resistance between Terminals W and B is therefore 120 Ω in general. The second connection is the first tap point, which corresponds to 198 Ω (RWB = 1/128 × RAB + RW = 78 Ω + 120 Ω) for programming code of 0x01 and so on. Each LSB data value increase moves the wiper up the resistor ladder until the last tap point is reached at 10,042 Ω (RAB – 1 LSB + RW). Regardless of which settings the part is operating with, care should be taken to limit the current conducted between any A and B, W and A, or W and B terminals to a maximum dc current of 5 mA and a maximum pulse current of 20 mA. Otherwise, degradation or possible destruction of the internal switch contact can occur. 96 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER Similar to the mechanical potentiometer, the resistance of the RDAC between the W and A terminals also produces a digitally controlled complementary resistance, RWA. When these terminals are used, the B terminal can be opened. Setting the resistance value for RWA starts at a maximum value of resistance and decreases as the data loaded into the latch increases in value. The general equation for this operation is RWA ( D) = 128 − D × R AB + RW 128 (5.6) Programming the potentiometer divider The digital potentiometer easily generates a voltage divider at Wiper W to Terminal B and Wiper W to Terminal A that is proportional to the input voltage at Terminal A to Terminal B. Unlike the polarity of VDD to GND, which must be positive, voltage across Terminal A to Terminal B, Wiper W to Terminal A, and Wiper W to Terminal B can be at either polarity. Figure 5.16 - Potentiometer Mode Configuration If ignoring the effect of the wiper resistance for the purpose of approximation, connecting the Terminal A to 30 V and the Terminal B to ground produces an output voltage at the Wiper W to Terminal B ranging from 0 V to 1 LSB less than 30 V. Each LSB of voltage is equal to the voltage applied across Terminals A and B divided by the 128 positions of the potentiometer divider. The general equation defining the output voltage at VW with respect to ground for any valid input voltage applied to Terminals A and B is VW ( D) = D VA 128 (5.7) A more accurate calculation that includes the effect of wiper resistance, VW, is 97 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER VW ( D) = RWB ( D) R ( D) V A + WA VB R AB R AB (5.8) Operation of the digital potentiometer in the divider mode results in a more accurate operation over temperature. Unlike when in rheostat mode, the output voltage in divider mode is primarily dependent on the ratio, not the absolute values, of the internal resistors RWA and RWB. Therefore, the temperature drift reduces to 5 ppm/°C. Wire serial bus digital interface The AD7376 contains a 3-wire digital interface (CS, CLK, and SDI). The 7-bit serial word must be loaded MSB first. The format of the word is shown in Figure 5.17. The positiveedge sensitive CLK input requires clean transitions to avoid clocking incorrect data into the serial input register. Standard logic families work well. When CS is high, the clock loads data into the serial register upon each positive clock edge (see Figure 5.18). Figure 5.17 - AD7376 Serial Data-Word Format Figure 5.18 - Wire Digital Interface Timing Diagram The AD7376 powers up at a random setting. However, the midscale preset or any desirable preset can be achieved by manipulating RS or SHDN with an extra I/O. When the reset (RS) pin is asserted, the wiper resets to the midscale value. Midscale reset can be achieved dynamically or during power-up if an extra I/O is used. 98 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER When the SHDN pin is asserted, the AD7376 opens SWA to let the Terminal A float and to short Wiper W to Terminal B. The AD7376 consumes negligible power during the shutdown mode and resumes the previous setting once the SHDN pin is released. On the other hand, the AD7376 can be programmed with any settings during shutdown. With an extra programmable I/O asserting shutdown during power up, this unique feature allows the AD7376 with programmable preset at any desirable level. Table 5.2 shows the logic truth table of all operation. table 5.2 - Input Logic Control Truth Table All digital inputs are protected with a series input resistor and a Zener ESD structure shown in Figure 5.19. These structures apply to digital input pins CS, CLK, SDI, SDO, RS, and SHDN Figure 5.19 - Equivalent ESD Protection Circuit All analog terminals are also protected by Zener ESD protection diodes, as shown in Figure 5.20. 99 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER Figure 5.20 - Equivalent ESD Protection Analog Pins The electrical schematic of the two digital potentiometer are shown in Figure 5.21 Figure 5.21 - Electrical schematic of the two digital potentiometer 5.1.5 DIP Switch In the node there is a DIP Switch used to store the address node. An A6E-8104 OMRON DIP switch has been used. This device is an 8-bit parallel load. The A6E-8104 contains eight pins connected to the PORTB of the PIC. Every PIN is put in an ON/OFF configuration. If the one PIN is put in ON configuration, the voltage 5V enters the one PIN of the PORTB of the PIC and this represents the high level (bit 1); if the same PIN is put in OFF configuration, the corrispective PIN of the PORTB of the PIC is put to ground and this represents the low level (bit 0). With this configuration it is possible to have 28 = 256 different ID. The Figure 5.22 shows the connection between the DIP Switch and the PORTB of the PIC. 100 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER Figure 6.18 - Electrical device of DIP SWITCH It is important to show that there is one resistance of 100 KΩ between every PIN of the DIP-Switch and the voltage VCC5. This solution is important to preserve the short circuit and has the same current in every PIN. To save space a resistor network 4609X-101-104LF by BOURNS company was used. The internal diagram block of the resistor network is shown in Figure 5.23 Figure 5.23 - 4609X-101-104LF block diagram The Resistance Tolerance is ±2 % and the power rating per resistor At 70 °C is 0.20 watt 5.1.6 Connection PIC18F458 - RF transceiver For the data wireless transmission a RF transceiver is used. The RF transceiver is a Easy Radio ER900TRS-02 by LPRS company [22]. There are four types of modules: The easyRadio (ER) ERx00TS Transmitter, ERx00RS Receiver, ERx00TRS transceiver and ERx00FHTRS Frequency Hopping Transceiver incorporate ‘easyRadio’ technology to provide high performance, simple to use radio 101 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER devices that can transfer data over a range of up to 250 metres Line Of Sight (LOS). Every ER module is available in two frequency versions: ER400 series (433-434MHz) & ER900 series (869.85MHz & 902-928MHz). Any other Easy-Radio Transceiver within range that ‘hears’ the transmission will decode the message and place the recovered data within a receive buffer that can then be unloaded to the receiving host for processing and interpretation. Transmission and reception are bidirectional half duplex i.e. transmit OR receive but not simultaneously. In Figure 5.24 the physical dimension of the RF transceiver is shown. Figure 5.24 - Physical Dimensions The connection between USART of the PIC and the RF transceiver module is shown in Figure 5.25 Figure 5.25 – Electrician connection of the RF module with PIC 102 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER The PIN of the ER900TRS-02 module are so connected: Pins Description 1 – Antenna It is connected to the antenna 2 – RF gnd It is connected to antenna gnd 3 – RSSI This pin is not connected, because in this basic configuration is not necessary the RSSI 4 – Busy out This pin is not connected, because the node communicates only with one PC master server so it is impossible that it is busy in other transmissions. 5 – SDO It is connected with the PIN 26 (RX) of the PIC18F458. This pin is used for transmission the ask of demand of data. 6 – SDI It is connected with the PIN 25 (TX) of the PIC18F458. This pin is used to take the data to be transmitted. 7 – Host This pin is not connected because the node communicates only with one Ready Input PC master server so it is impossible that is busy in other transmissions. 8 – Vcc It is connected with a positive supply 5 V. 9 – Ground It is connected to ground. In the Table 5.2 the timing specification applies to all Easy-Radio modules are shown. Table 5.2 - Timing specification Notes 1. Data is inverted i.e. Start Bit is logic low. The inputs are intended for direct connection to a microcontroller UART or to RS232 inputs and outputs via an 103 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER RS232 Level translator such as a Maxim MAX232, which invert the logic of the RS232 signals. This allows direct connection to, for example a Microcontroller UART. The data rate is user programmable (Default 19200 baud) and may differ between individual units within a system. (See Application Circuit diagram for logic level to RS232 interface figure 11). 2. 1 start, 8 data, 1 stop = 10 bits @ 104uS/bit = 0.52mS/character at 19200 Baud. (Default) a. Some Custom BAUD rates require 2 stop bits, otherwise some characters may be lost. b. If parity is used, substitute in the above calculation using 11 bits. 3. The ‘End of Data’ delay is fixed at twice the character time. 4. A fixed package overhead of 13.2mS is added to all packets. 5. The buffer size is limited to 180 bytes. Sending more than 180 bytes will cause loss of data. a. CTS pin will go high 2 bytes before the buffer is full. This allows characters already sent to be accepted by the ER module. 5.1.6.1 Message Format The Users Data is enclosed within a ‘packet’ that has the following format and timing: The additional data sent within a packet imposes a fixed ‘overhead’ on the time taken to send the users data. The ‘airtime’ required to send, for example, 32 bytes of User Data can be calculated as: 104 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER 5mS + (4 x 800uS) + (32 x 800uS) = 33.8mS total This then allows the total ‘End to End’ (Host to Host) message time for 32 Bytes of User Data sent at 19200 baud to be calculated: In addition there may be variable handshake delays (dependant upon the host) whilst the hosts test the handshake lines. Note that the host to Easy-Radio module ‘load’ and ‘unload’ times are dependant upon the data rate chosen for the serial interface. 5.1.6.2 Addressing There is no hardware or software ‘addressing’ incorporated within the Easy-Radio Transceivers as requirements will vary dependant upon the users’ application. It is however very easy to embed addressing and other information within the message. A typical user message (often called a ‘telegram’) might comprise the following format: where 105 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER There are many standard protocols (e.g. Ethernet) that are necessarily complicated by the need to provide multiple universal ‘services’. Most applications do not require or cannot be burdened with the ‘overhead’ of these protocols and a much simplified subset will usually suffice. The essence of ‘Easy-Radio’ is to provide the reliable transport of serial data over a radio link so that the user can concentrate their efforts on the application. 5.1.7 Antenna The RF transceiver can be used with the various common types of antenna that match the 50. RF Input/Output such as a monopole (whip), helical or PCB/Wire loop antennas. Monopole antennas are resonant with a length corresponding to one quarter of the electrical wavelength (λ/4). The monopole or Whip Antenna are just about universally used for Very High Frequency radio transmission and reception. Whip antennas are also sometimes used for Medium Frequency and High Frequency transmission and reception. Helical antennas are also resonant and generally chosen for their more compact dimensions. They are more difficult to optimise than monopole antennas and are critical with regard to surrounding objects that can easily ‘de-tune’ them. They operate most efficiently when there is a substantial ground plane for them to radiate against. Wire or PCB Loop antennas are the most compact antennas but are less effective than the other types. They are also more difficult to design and must be carefully ‘tuned’ for best performance. The antenna used for the transceiver is an ANT-900MS of the LPRS [32]. It is a 900MHz monopole antenna with straight male SMA connector. The dimensions are drawn in Figure 5.26 106 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER Figure 5.26 – Physical dimensions of the monopole antenna The electrical characteristics are • Resonant Frequency: 900MHz • Return Loss: -17 dB or less • Radiation Pattern: Omni Directional • Polarization: Vertical • Standing Wave Ratio(S.W.R.): = 1.7 • Insulation resistance: 500Mohm @ DC 500V The general characteristics are • Storage Temperature: -30° to + 75° Figure 2 • Operating Temperature: -30° to + 75° • Vibration Test: There shall be no defects in appearance or the mechanical and electrical functions after the antenna being tested by regular mounting device under the following conditions: - Displacement: ±5° of axis original position - Duration: 1000 cycles/minute - Time: 5 minutes - iv) Shock Resistance: Satisfy the electrical and mechanical characteristics after drop down - with 100g upon rubber block The physical monopole antenna is shown in Figure 5.27. 107 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER Figure 5.27 – Physical dimensions of the monopole antenna 5.1.8 Voltage regulator All previous circuits have different power supply, exactly 3 type of power supply: 15V (digital potentiometer, operational amplifier), 5V (PIC18F458, RF module, ID node) and 3.3V (temperature sensor). This voltages are not directly applied to the circuit, exactly for the 15V (this is the voltage of the battery), but two voltage regulators are used, as it is shown in Figure 5.28. (a) (b) Figure 5.28 - Electrical circuit of the two voltage regulators: (a) 5V voltage regulator and (b) 3.3 V voltage regulator. 108 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER The principal element of the circuit (a) is the LF50CV. This element converts the 15V in 5V. A 100 nF and 22 uF capacitors have been applied at the supplies to minimize transient disturbances and filter low frequency ripple. The principal element of the circuit (b) is the LF33CV. This element converts the 5V in 3V. A 100 nF and 22 uF capacitors have been applied at the supplies to minimize transient disturbances and filter low frequency ripple. It is possible to convert directly 15V in 3.3V, but to save power dissipation it is better to convert 5V in 3.3V according to the power dissipation formula: Pd = (VIN – VOUT) x I Where Pd is the power dissipation in Watt, VIN is the voltage in input, VOUT is the voltage in output and I is the current. The LF50CV and LF33CV is made by STMicroelectronics and are of the LF00 series. The LF00 series are very Low Drop regulators available in PENTAWATT, TO-220, TO220FP, DPAK and PPAK package and in a wide range of output voltages (see Figure 5.29). Figure 5.29 – Connection diagram (top view) of the different package. 109 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER The very Low Drop voltage (0.45V) and the very low quiescent current make them particularly suitable for Low Noise, Low Power applications and specially in battery powered systems. In the 5 pins configuration (PENTAWATT and PPAK) a Shutdown Logic Control function is available (pin 2, TTL compatible). This means that when the device is used as a local regulator, it is possible to put a part of the board in standby, decreasing the total power consumption. In the three terminal configuration the device has the same electrical performance, but is fixed in the ON state. It requires only a 2.2 µF capacitor for stability allowing space and cost saving. In the system was used the TO-220 package for both voltage regulators LF50CV and LF33CV, Infect LF is the family, 50 or 33 is the voltage in output (5.0V and 3.3 volt) and CV is the code of the package [33]. 5.1.9 Connectors The second PCB uses 3 connectors shown in Figure 5.30 Figure 5.30 – electrician schematic of the second PCB connectors The connectors P1, P2, P3, P4 and P5 have the following functions: • P1 is the connector for the power supply, where VCC is 15V and VEE is -15V; • P2 is the connector to change the division scaling factor of the two multipliers through the two digital multimeters. Vcomp1 and Vcomp2 are the analog outputs of the digital multimeters; 110 CHAPTER 5 • HARDWARE REMOTE NODE AND INTERFACE CCP SERVER P3 is the connector to read the two DC components (phase and quadrature) in output of the inductive conductivity sensor. These two DC components will be processed by a microcontroller which, together with a temperature sensor, will extracts the conductivity of the water. 5.2 Building PCB node After the schematic editor, the next step has been to convert the project in a PCB. As the first PCB (Hardware inductive sensor interface) the program Altium Designer 6 has been used again, because it has this possibility; the components in the schematic have been converted in physical dimensions to be put in the PCB and the ways of connection have been drawn with all the components. The PCB has been built in the IST (Instituto Superior Técnico) laboratories. In Figure 5.31 the PBC bottom layer is shown. (a) (b) Figure 5.31 - Layers of the PCB: (a) without ground, (b) with the ground for the final print 111 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER In Figure 5.32 the PCB bottom printer without any electronic components is shown. Figure 5.32 - PCB bottom printer The PCB top printer with all electronic components is depicted in Figure 5.33. Figure 5.33 - PCB top printer with all electronic components 5.3 Bill of materials 2° PCB In the table 5.3 there is a list of all the components and materials used to build the second PCB. This list is composed of the name of the component, model and company, the name 112 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER in the schematic, the value if it is applicable, the quantity and the price in euro updated at September 2006 by Farnell Catalogue 2006. Picture Component/Model/Company Designator Value Capacitor / MULTICOMP C1, C3, C5, C6, C8, C10, C12, C14, C15, C16, C17, C19, C21 Polarized Capacitor (Axial) / C2, C4, MCGPR25V226M5X11/ MULTICOMP C7, C9, C11, C13, C18, C20, C22 High Conductance Fast Diode / Diode D1, D2, 1N4148 / MULTICOMP D3, D4, D5, D6 Resistor / MULTICOMP R1, R2, R3 Microcontroller / PIC18F458 / Microchip OP-AMP / KA741 / FAIRCHILD SEMICONDUCTOR Quantity Price € Total € 1nF, 22pF, 100nF 13 0,092 1,196 9 0,055 0,495 6 0,017 0,102 3 0.032 0,096 1 4,78 4,78 1 0,57 0,57 1 0,18 0,18 1 0,97 0,97 1 0,22 0,22 1 1,14 1,14 1 23,85 23,85 1 3,47 3,47 1 4,75 4,75 22uF 10K, 22K U3 U4 RESISTOR NETWORK / 4609X-101104LF / BOURNS DIP Switch / MCDS08 / MULTICOMP 100K S1 IC SOCKET, DIL 0.3" 8WAY / 2227MC-08-03-18 / MULTICOMP IC SOCKET, DIL 0.6" 40WAY / 2227MC-40-06-05 / MULTICOMP RF-Receiver / EASY RADIO ER900TRS / LPRS U5 Coaxial Connector Type: SMB / 19-461-TGG / MULTICOMP P9 Whip Antenna / ANT-900MS / LPRS 113 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER Voltage Regulator / LF50CV / STMICROELECTRONICS U1 Voltage Regulator / LF33CV / STMICROELECTRONICS U2 TERMINAL BLOCK VERTICAL / 3-Pin CAMDEN ELECTRONICS / TERMINAL BLOCK VERTICAL / 2-Pin CAMDEN ELECTRONICS / 1 1,41 1,41 1 1,41 1,41 3 0,46 0,46 1 0,31 0,31 1 1,25 1,25 P1, P3, P4 P2 Temperature Sensor / AD22103 / Analog Device Total 47 table 5.3 - Bill of materials 2° PCB 114 46,66 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER 5.4 Electrical circuit of the CCP interface In this section the principal parts of the hardware of the CCP interface will be analyzed. In particular, the max232 and the bridge RF transceiver-max232-RS232 will be explained. The general structure of the transceiver is shown in Figure 5.34. Power Supply 9 Volt 5 Volt SDO / T1IN SDI / R1OUT MAX232 I/O Antenna RF TRANSCEIVER Voltage regulator SDO / T1OUT SDI / R1IN Figure 5.34 - Block diagram of the CCP interface It is composed of a RF transceiver that communicates with a PC by RS232 port. For the connection of the RF transceiver with the pc a connector with 9 PIN and a MAX232 are required. The MAX232 is required because the PC and the RF module have different values of voltage for the high and low level. Figure 5.34 shows the “schematic” of the PCB based on the block diagram shown in Figure 5.35. The schematic is composed by the following parts and components: • Bridge RF module - Max232 - Port RS232 • Voltage regulator • Connectors 115 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER Figure 5.35 - Block diagram of the CCP interface 116 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER 5.4.1 Bridge RF transceiver - Max232 – RS232 port In Figure 5.36 is shown the electrician connection between the RS232 port of the PC master server and the RF transceiver. Figure 5.36 - Bridge RF transceiver - Max232 – RS232 port The ERx00TRS uses crystal controlled synthesisers to accurately define transmit and receive frequencies incorporating RS232 protocols. The RS232, also more commonly known as the serial, specifications specifies that a logic '1' is represented by +12.5V and a logic '0' is represented by -12.5V. This obviously presents many problems for RF transceiver that are running at +5V. That is where the level translator comes into play; it translates -12.5V to 0V and 12.5V into 5V, standard TLL logic levels. The schematic 6.31 shows the simplicity of the design by using one of Maxim IC’s level translators; the pin 5 of the RF transceiver (data out) is connect at the pin 2 of the RS232 port (Receive Data) and the pin 6 of the RF transceiver (data in) is connect at the pin 3 of the RS232 port (Transmit Data). The MAX232 is a dual driver/receiver that includes a capacitive voltage generator to supply EIA-232 voltage levels from a single 5-V supply. Each receiver converts EIA-232 117 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER inputs to 5-V TTL/CMOS levels. These receivers have a typical threshold of 1.3 V and a typical hysteresis of 0.5 V, and can accept ±30V inputs. Each driver converts TTL/CMOS input levels into EIA-232 levels. In Figure 5.37 it is shown the pins of the MAX232 and the basic configuration [34]. EW) (a) (b) Figure 5.37 – Max232: (a) Pins, (b) basic configuration 5.4.2 Voltage regulator All previous circuits require 5V power supply. A voltage regulator LF50CV is used. It is shown in Figure 5.38. Figure 6.33 - Electrical circuit of the 5V voltage regulator The principal element of the circuit is the LF50CV. This element converts the Vcc power supply in 5V. A 100 nF and 22 uF capacitors have been applied at the supplies to minimize transient disturbances and filter low frequency ripple. 118 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER 5.5 Building PCB master server After the schematic editor, the next step has been to convert the project in a PCB. As the first and the second PCB the program Altium Designer 6 has been used again. The PCB has been built in the IST (Instituto Superior Técnico) laboratories. In Figure 5.39 the PBC bottom layer is shown. (a) (b) Figure 5.39 - Button layer of the PCB: (a) without ground, (b) with the ground for the final print In Figure 5.40 the PCB bottom printer without any electronic components is shown. Figure 5.40 - PCB bottom printer 119 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER The PCB top printer with all electronic components is depicted in Figure 5.41. Figure 5.41 - PCB top printer with all electronic components 5.6 Bill of materials 3° PCB In the table 5.4 there is a list of all the components and materials used to build the third PCB. This list is composed of the name of the component, model and company, the name in the schematic, the value if is applicable, the quantity and the price in euro updated at September 2006 by Farnell Catalogue 2006. Picture Price € Total € Component/Model/Company Designator Value Quantity Capacitor / MULTICOMP C1, C3, C7 100nF, 100pF 3 0,092 0,276 6 0,055 0,33 1 1,36 1,36 1 0,38 0,38 Polarized Capacitor (Axial) / C2, C4, MCGPR25V226M5X11/ MULTICOMP C5, C6, C8, C9 SOCKET, D PCB R/A 9 WAY / 788750-1 / TYCO ELECTRONICS SOCKET LOW VOLTAGE 1.9MM, 2Pin / 120 22uF J1 P1 CHAPTER 5 HARDWARE REMOTE NODE AND INTERFACE CCP SERVER Coaxial Connector Type: SMB / 19-461-TGG / MULTICOMP P9 Voltage Regulator / LF50CV / STMICROELECTRONICS U1 RF-Receiver / EASY RADIO ER900TRS / LPRS U2 RS-232 / MAX232AESE / TEXAS INSTRUMENTS U3 IC SOCKET, DIL 16 WAY / 816AG11D-ESL-LF / TYCO ELECTRONICS Whip Antenna / ANT-900MS / LPRS Total Table 5.4 - Bill of materials 3° PCB 121 1 3,47 3,47 1 1,41 1,41 1 23,85 23,85 1 0,84 1 0,983 0,983 1 17 4,75 0,84 4,75 37,65 Chapter 6 Testing and Characterization of the Inductive Sensor As it has been seen in chapter 1, the conductivity sensor exhibits a non-trivial dependence on the water temperature that requires calibrating techniques to ensure good accuracy, in fact almost all parameters (physical and chemical), used for in-situ water quality monitoring of rivers and seas, are measured using sensors that have characteristics highly sensitive with temperature. This chapter focuses on the testing and the characterization of the inductivity conductivity sensor mounted on the PCB, using a low cost testing bath with automated controlled temperature to characterize sensors for in-situ water quality monitoring built in the Instituto de Telecomunicações (it) laboratories of lisboa [28]. This system proved to be an adequate tool to calibrate almost any type of sensors to be used in water quality monitoring. It can be used to study the characterization and use of several sensors, namely, ion selective electrodes (ISE) that are an important tool to determine a large number of heavy metal ions concentrations in water. 6.1 The Low-Cost Temperature Controlled System: system description The Low-Cost Temperature Controlled System to Test and Characterize Sensors is a system to characterize in general the sensors used for the quality monitoring. In Figure 6.1 the block diagram of the automated temperature controlled bath is shown. The bath has a maximum capacity of 14 liters. Since it is to be used for 122 CHAPTER 6 TESTING AND CHARACTERIZATION OF THE INDUCTIVE SENSOR characterizing sensors for water quality monitoring the temperature range was specified to be in the 10 to 30°C interval. In order to control the temperature a heating/cooling thermoelectric pump (TE) based on Peltier modules and a proportional-integral-derivative (PID) controller implemented in LabVlEW are used. To improve the heat distribution inside the bath and to ensure a good temperature homogeny a shaker is used. The shaker consists on two propellers mechanically connect to a small DC motor which is outside the bath. Figure 6.1 - Block diagram of the testing system. Other elements presented in the system are the temperature sensors, a data acquisition board (DAQ) that acquires the voltages associated to the conditioning circuits (CC - PT100) and (CC - AD) and a IEEE 488.2 interface board (lEEE488.2) used to control the power supply of the thermoelectric pump. 6.1.1 The container The 14-liter plexiglas container was built taking into account the need to achieve a quick homogeneity of the liquid temperature. To achieve this, a shaker was inserted into the bath to force liquid circulation and thus achieve faster temperature homogeneity. To improve the water circulation, the shape of the container resembles a oval speed track to remove sharp edges and dead zones. The material of the container are chose in order to minimize heat transfers with the ambient environment. 123 CHAPTER 6 TESTING AND CHARACTERIZATION OF THE INDUCTIVE SENSOR In one of the flat walls of the container there are four openings where copper boards are placed. Outside the bath, in each board a thermoelectric module is thermally and physically attached to the container structure. Inside the bath, aluminium heat exchangers improve the heat transfers between the thermoelectric modules and the liquid - Figure 6.2. Figure 6.2 - Bath with heat exchangers in the cold surface each TE. 6.1.2 Heating/cooling thermoelectric pump To select the thermoelectric device (TE) three specific system parameters must be determined: the cold surface temperature, Tc; the hot surface temperature, TH and the amount of heat to be absorbed at the cold surface of the TE, Qc. Four thermoelectric devices CP 1.4-127-06L from MELCOR were used. Each device has 127 thermocouples electrically connected in series, and thermally in parallel. Their specifications are: maximum temperature between cold and the hot junctions is ΔTmax=67°C; input current for ΔTmax is 6A; input voltage for ΔTmax=67°C is 15.4V; maximum heat absorbed by the cold junction with ΔT=0°C is 51.4W. As stated, the temperature range of the bath was specified as [10; 30] (°C). Since it is to be used indoors, most of the times the thermoelectric device will operate to cool the liquid. If the bath is in direct contact with the cold surface of the thermocouple, the desired bath temperature can be considered equal to the temperature of the cold surface of the TE. To get better results, a heat exchanger on the cold surface of the 124 CHAPTER 6 TESTING AND CHARACTERIZATION OF THE INDUCTIVE SENSOR TE (inside the bath) is employed as depicted in Figure 6.2. This may cause Tc to be several degrees colder than the bath temperature. In order to define the temperature of the hot surface, besides the temperature of the ambient environment, the efficiency of the heat exchanger that is between the hot surface and the ambient environment needs to be analyzed. To cool the hot junction with water, aluminum modules where the water is forced to circulate in internal waterways on contact with the TE hot surface, allowing an effective cooling were built. The water circulation is achieved with a small pump. There is a physical support with the water inputs and outputs to each module as represented in Figure 6.4. Figure 6.4 -Aluminium modules mounted on the outside surface of the TE. The white arrows represent the water entry into the modules while the black arrows represent the output flow. 6.1.3 Measuring System Four AD22103 temperature sensor (see paragraph 6.2.2 fore more details about this sensor) are used to assess the temperature of the water in the bath. The sensors are interfaced to the PC by conditioning circuits (CC) and a multichannel 12bit NI-PCI 6024E data acquisition board. In order to improve the final resolution, the conditioning circuits were implemented to produce output voltages in the ADC range +/-5V of the board for the temperature limits of the system. In the +5V the value of the least significant byte (LSB) of the ADC is 2.44 mV. The sensor AD22103KT was chosen because its low cost, its good sensor linearity, its temperature range and its good response time. 125 CHAPTER 6 TESTING AND CHARACTERIZATION OF THE INDUCTIVE SENSOR 6.1.4 PID controller To ensure accurate thermoelectric temperature control, a digital proportionalintegral-derivative (PID) controller was implemented in LabVIEW. The purpose of the controller is to measure the temperature of the bath, compare it with the desired value (set point) and generate a control signal (input current far the TE modules) to drive the bath temperature towards the set point. The parallel PID algorithm implemented is defined by t S (t ) = PE (t ) + R ∫ E (t )dt + D 0 dE (t ) dt (6.1) where S(t) is the control variable (input current for the TE modules), E(r) is the error between the user defined set point (desire temperature value for the bath) and the measured process variable (temperature bath). Parameter P defines the weight of the proportional term, while parameters R and D refer to the integral and derivative terms. These controlled parameters were obtained with the Ziegler-Nichols method and adjusted under real working conditions. The final parameters are P=54,42 A/°C and R=0.636 A/(°Cs). PID controller derivate component (D) is not used do to the instability caused in controller’s output. After computing the output value of the controller, its value is limited to the maximum and minimum values of the controller operation. This means the maximum input current for each TE module: 4.5 A. In Figure 6.5 the front panel of the LabVIEW application built to implement the control algorithm is shown. 126 CHAPTER 6 TESTING AND CHARACTERIZATION OF THE INDUCTIVE SENSOR Figure 6.5 - Front panel of the LabVIEW application 6.2 Experimental characterization 6.2.1 Experimental setup For characterizing the sensor with the Hardaware Sensor Interface we have used: - a variable resistance; - distillate water in which NaCl has been added to increase the conductivity; - 3 different conductivity solutions; - an automated temperature controlled bath system; - a commercial conductivity analyzer. The variable resistance has been used to simulate the conductivity variation in the water and to see the variation of the two voltage components in output of PCB (Exit1- component in phase and Exit2 – component in quadrature). The resistance have a range between 0 Ohm and 1000 Ohm. Figure 6.6 – View of the variable resistance by LLOYD instrumentation 127 CHAPTER 6 TESTING AND CHARACTERIZATION OF THE INDUCTIVE SENSOR The distillate water, in which NaCl has been added to increase the conductivity, has been used to simulate the conductivity variation in the water and to see the variation of the two voltage components in output of PCB (Exit1- component in phase and Exit2 – component in quadrature). The automated temperature controlled bath system (see previous paragraph) has been used to characterize the sensor by seeing the two voltage component in output to PCB (Exit1 and Exit2) at the variation of the temperature and with 3 different conductivity solutions. In Figure 6.7 the system ready to receive the inductive conductivity sensor and to start up the measure is shown. Figure 6.7 – Views of the automated temperature controlled bath system 128 CHAPTER 6 TESTING AND CHARACTERIZATION OF THE INDUCTIVE SENSOR To measure temperature, a three terminal sensor (AD22103) with a temperature coefficient of 28 mV/°C have been used. The commercial conductivity analyzer has been used as reference system for the measure of the conductivity and the temperature compensation. It has been used for the calibration procedure. 6.2.2 Experimental Characterization and Discussion Before starting up the experimental measure, the correct working of the PCB has been tested. We have measured if the frequency and the amplitude of the sine and cosine wave signals were equivalent to the project value. After that, the next measure has been to control if the signal in output of the two multipliers had a double frequency compared with the frequency in input. After checking the correct PCB working, the next step has been the measure of the variation of the two voltage components in output to PCB (Exit1- component in phase and Exit2 – component in quadrature), when the inductive sensor has been connected to the PCB. The multipliers configuration was put in fixed scale configuration (scale factor of 2 for the component in phase and 1 for the component in quadrature) The variation of the water conductivity has been simulated with a variable resistance. The experimental values, obtained by using the variable resistance, are presented in Figure 6.8 129 CHAPTER 6 TESTING AND CHARACTERIZATION OF THE INDUCTIVE SENSOR EXIT 1 - component in phase (scale factor 2V) 5 10 4,5 11 12 13 14 15 4 Output Voltage [V] 3,5 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 3 2,5 2 40 1,5 50 60 70 80 90100 1 0,5 200 300 400 0 0 200 500 400 600 700 600 800 900 800 1000 1000 Resistance [Ω] (a) EXIT 2 - component in quadrature (scale factor 1V) 4,5 4 3,5 Output Voltage [V] 3 2,5 10 11 12 13 1421 1522 1623 1724 1825 1926 2027 28 29 3040 50 2 60 1,5 70 80 90 100 1 200 0,5 300 400 500 600 700 800 900 0 Resistance [Ω] (b) Figure 6.8 - Variation at the two voltage components in output to PCB at the variation of the resistance: (a) component in phase, (b) component in quadrature In Figure 6.9 the two voltage components at the variation of conductivity of the water are shown. Now the variation of conductivity of the water is simulated adding Nacl (with an increasing step of 2.5 grams) to 2 Liters of distillate water at the temperature of 25°C. The range of the conductivity is 5-50 [mS/cm] because this is the possible range in the river estuary. 130 1000 CHAPTER 6 TESTING AND CHARACTERIZATION OF THE INDUCTIVE SENSOR EXIT 1 - component in phase 3 2,5 55,4 53,7 52,1 50,5 48,8 47 45,8 44,1 42,3 40,6 38,8 Output Voltage [V] 2 36,9 35,3 33,6 1,5 31,7 29 27,3 25,7 1 23,8 21 19,2 17,09 15,21 0,5 12,79 11,35 9,37 5,2 7,12 2,75 0 0 10 20 30 40 50 60 Conductivity [mS/cm] (a) EXIT 2 - component in quadrature 6 5 31,7 Output Voltage [V] 4 21 19,2 17,09 23,8 52,153,755,4 47 48,850,5 44,145,8 40,642,3 36,9 38,8 33,635,3 29 27,3 25,7 15,21 12,79 11,35 3 9,37 7,12 5,2 2 2,75 1 0 0 10 20 30 40 50 60 Conductivity [mS/cm] (b) Figure 6.9 - The two voltage components at the variation of conductivity of the water: (a) component in phase, (b) component in quadrature In Figure 6.10 the graphics of the Figure 6.9 are shown but on the X axis there is the resistivity. 131 CHAPTER 6 TESTING AND CHARACTERIZATION OF THE INDUCTIVE SENSOR EXIT 1 - component in phase 3 2,5 18,1 18,6 19,2 19,8 20,5 21,3 21,8 22,7 23,6 24,6 25,8 Output Voltage [V] 2 27,1 28,3 29,8 31,5 1,5 34,5 36,6 38,9 42,0 1 47,6 52,1 58,5 65,7 78,2 88,1 106,7 140,4 0,5 192,3 363,6 0 0,0 100,0 200,0 300,0 400,0 500,0 600,0 700,0 800,0 900,0 1000,0 700,0 800,0 900,0 1000,0 Resistivity [Ohm×cm] (a) EXIT 2 - component in quadrature 5,5 18,6 18,1 19,2 19,8 20,5 21,3 21,8 22,7 23,6 24,6 25,8 27,1 28,3 29,8 31,5 34,5 36,6 38,9 42,0 47,6 52,1 58,5 5 4,5 Output Voltage [V] 4 3,5 65,7 78,2 88,1 3 106,7 140,4 2,5 192,3 2 363,6 1,5 1 0,0 100,0 200,0 300,0 400,0 500,0 600,0 Resistivity [Ohm×cm] (b) Figure 6.10 - The two voltage components at the variation of resistivity of the water: (a) component in phase, (b) component in quadrature By the experimental value shown in Figure 6.8 and 6.9 using the commercial conductivity analyzer, it is possible to find the “cell constant”. This value Kc only depends on the geometric shape. This geometry factor was assessed using a calibration procedure. However an estimated value was obtained previously by using the finite element method [2]. 132 CHAPTER 6 TESTING AND CHARACTERIZATION OF THE INDUCTIVE SENSOR The calibration procedure has used a commercial conductivity analyzer. It is possible to find the experimental cell constant value by the following formula: Rw = Kc (6.2) σ where Kc is the cell costant [m-1], Rw is the resistance of water simulated by variable resistor [Ω] and σ is the conductivity of the water calculated by the commercial conductivity analyzer 50 [S/m] The value Kc = 140 m-1 has been obtained. This value is a little bit different from the value calculated by the finite element method (Kc = 110 m-1); as a matter of fact, in order to put the sensor in the “bath”, the plastic container dimensions of the sensor have been made smaller. Temperature compensation Another experimental characterization has been the effect of temperature. The effect of temperature is also important when an electrical conductivity measurement of a solution must be done. A solution of a higher temperature will present a higher quantity of ions dissociated, therefore a higher concentration of electric charges and as consequence conductivity will raise. The degree to which temperature affects conductivity varies from solution to solution and can be calculated using the following formula: σ T = σ Tcal [1 + α(T-Tcal)] Where σ T (6.3) = conductivity at any temperature T in °C, σ Tcal = conductivity at calibration temperature Tcal in °C and α = temperature coefficient of solution at Tcal in °C. The automated temperature controlled bath system has been used to characterize the sensor seeing the two voltage components in output to PCB (Exit1 and Exit2) at the temperature variation and with 3 different conductivity solutions. The multipliers 133 CHAPTER 6 TESTING AND CHARACTERIZATION OF THE INDUCTIVE SENSOR configuration was put in manual potentiometer scale configuration and the scale factor is 1 for the component in phase and 1 for the component in quadrature. In Figure 6.11 dots represent the conductivity as a function of temperature for different values of the solution conductivity measured with the commercial conductivity analyzer. In Figure 6.12 dots represent the DC voltage component in phase as a function of temperature for different values of the solution conductivity measured in output of the hardware inductive sensor interface. For every value the linear temperature compensation formula (6.3) has been used. The value of NaCl diluted in every solution has been shown in table 6.1. Total Concentration NaCl[g/l] NaCl Saled water I 0,05N 2,94064 Saled water II 0,1N 5,88208 Saled water III 0,2N 11,76392 table 6.1 - Value of NaCl diluted in every solution CONDUCTIVITY vs TEMPERATURE 30 Conductivity [mS/cm] 25 20 15 10 5 0 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 Temperature [ºC] SALED WATER I (0,05N) SALED WATER II (0,1N) SALED WATER III (0,2N) Figure 6.11 – Temperature compensation for different values of the solution conductivity measured with the commercial conductivity analyzer. 134 CHAPTER 6 TESTING AND CHARACTERIZATION OF THE INDUCTIVE SENSOR DC COMPONENT IN PHASE vs TEMPERATURE 4 3,5 Output Voltage [V] 3 2,5 2 1,5 1 0,5 0 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 Temperature [ºC] SALED WATER I (0,05N) SALED WATER II (0,1N) SALED WATER III (0,2N) Figure 6.12 - Temperature compensation of the DC voltage component in phase for different values of the solution conductivity From the values described above a temperature coefficient of 2,02%/°C at 25°C has been calculated. The DC voltage component in quadrature has not been tested because it is not important to extract information about the conductivity. 135 Conclusions A remote node for the water quality to measure the electrical conductivity of the salty water has been developed, constructed and characterized in IT laboratory of Lisbon. A number of these sensors will be placed in the river Tagus estuary near Lisbon. The array of sensors will work autonomously. Each sensor provided with a microprocessor to automate the measuring process and to control the transmission of data to a central point where the collected information will be processed. On the basis of the result shown above, the future development can be: - testing of other characteristics that are not yet implemented; - adding new functionalities to the node; - upgrade the system at some levels like sensors integration with more parameters like heavy metals and nutrients; - create a net that allows costs containment; - introducing a different type of wireless communication. Besides, the next step of integration is the remote control of the device with the use of a GSM/GPRS system. 136 APPENDIX A Appendix A MpLAB IDE MPLAB IDE is a software program that runs on a PC to develop applications for Microchip microcontrollers. It is called an Integrated Development Environment, or IDE, because it provides a single integrated .environment. to develop code for the Microchip Technology Incorporated PICmicroncontroller (MCU) and dsPIC digital signal controller (DSC) families. The components of MPLAB IDE are: • Project Manager - The project manager provides integration and communication between the IDE and the language tools. • Editor - The editor is a full-featured programmer's text editor that also serves as a window into the debugger. • Assembler/Linker and Language Tools - The assembler can be used stand- alone to assemble a single file, or can be used with the linker to build a project from separate source files, libraries and recompiled objects. The linker is responsible for positioning the compiled code into memory areas of the target microcontroller. • Debugger - The Microchip debugger allows breakpoints, single stepping, watch windows and all the features of a modern debugger for the MPLAB IDE. It works in conjunction with the editor to reference information from the target being debugged back to the source code. • Execution Engines - There are software simulators in MPLAB IDE for all PICmicro MCU and dsPIC DSC devices. These simulators use the PC to simulate the instructions and some peripheral functions of the PICmicro MCU and dsPIC DSC devices. Optional in-circuit emulators and in-circuit debuggers are also available to test code as it runs in the applications hardware. 137 APPENDIX A Optional components can be purchased and added to the MPLAB IDE are: • Compiler Language Tools - MPLAB C18 and MPLAB C30 C compilers from Microchip provide fully integrated, optimized code. Along with compilers from HI-TECH, IAR, microEngineering Labs, CCS and Byte Craft, they are invoked by the MPLAB IDE project manager to compile code that is automatically loaded into the target debugger for instant testing and verification. • Programmers - PICSTART Plus, PICkit 1 and 2, PRO MATE II, MPLAB PM3 as well as MPLAB ICD 2 can program code into target devices. MPLAB IDE offers full control over programming both code and data, as well as the Configuration bits to set the various operating modes of the target microcontrollers or digital signal controllers. • In-Circuit Emulators - MPLAB ICE 2000 and MPLAB ICE 4000 are full- featured emulators for the PICmicro MCU and dsPIC DSC devices. They connect to the PC via I/O ports and allow full control over the operation of microcontroller in the target applications. • In-Circuit Debugger - MPLAB ICD 2 provides an economic alternative to an emulator. By using some of the on-chip resources, MPLAB ICD 2 can download code into a target microcontroller inserted in the application, set breakpoints, single step and monitor registers and variables [35]. 138 APPENDIX A Figure A.1 - MPLAB® IDE DESKTOP The project manager organizes the files to be edited and other associated files so they can be sent to the language tools for assembly or compilation, and ultimately to a linker. The linker has the task of placing the object code fragments from the assembler, compiler and libraries into the proper memory areas of the embedded controller, and ensure that the modules function with each other (or are .linked.). This entire operation from assembly and compilation through the link process is called a project build. From the MPLAB IDE project manager, properties of the language tools can be invoked differently for each file, if desired, and a build process integrates all of the language tools operations. 139 APPENDIX A Figure A.2 - MPLAB® IDE PROJECT MANAGER The source files are text files that are written conforming to the rules of the assembler or compiler. The assembler and compiler convert them into intermediate modules of machine code and placeholders for references to functions and data storage. The linker resolves these placeholders and combines all the modules into a file of executable machine code. The linker also produces a debug file which allows MPLAB IDE to relate the executing machine codes back to the source files. A text editor is used to write the code. It is not a normal text editor, but an editor specifically designed for writing code for Microchip MCUs. After the code is written, the editor works with the other tools to display code execution in the debugger. After the application has been debugged and is running in the development environment, it needs to be tested on its own. A device can be programmed with the in-circuit debugger or a device programmer. As programmer it is used the PICSTART PLUS Development programmer. 140 APPENDIX A The PICSTART Plus is a Microchip microcontroller development programmer that enables you to program user software into PICmicro microcontroller devices. In Figure A.3 is shown a view of programmer. Figure A.3 - A view of programmer 141 APPENDIX B Appendix B C18 C compiler C18 C Compiler is a cross-compiler that runs on a PC and produces code that can be executed by the Microchip PIC18XXXX family of microcontrollers. C18 C compiler makes development of embedded systems applications easier because it uses the C standard language. Like an assembler, the C18 C compiler translates humanunderstandable statements into ones and zeros for the microcontroller to execute. Unlike an assembler, the compiler does not do a one-to-one translation of machine mnemonics into machine code. C18 C compiler and its associated tools, such as the linker and assembler, can be invoked from the command line to build a .HEX file that can be programmed into a PIC18XXXX device. C18 and its other tools can also be invoked from within MPLAB IDE [36, 37]. The Figure B.1 shows the step from the C-file to the chip programming. Figure B.1 - Step from the C-file to the chip programming 142 APPENDIX C Appendix C Altium Designer 6 Altium Designer brings a complete electronic product development environment to your PC’s Desktop, providing multi-document editing and full customization of the design workspace. Altium Designer provides a unified electronic product development environment, catering for all aspects of the electronic development process, including: • System Design and Capture • Physical PCB Design • FPGA Hardware Design • Embedded Software Development • Mixed-Signal Circuit Simulation • Signal Integrity Analysis • PCB Manufacturing • FPGA system implementation and debugging (when working with a suitable FPGA development board, such as an Altium NanoBoard). All of these design areas are intrinsic parts of a single, cohesive system, built on Altium Designer's Design Explorer (DXP) integration platform. The extent of this unified system, in terms of the features and functionality available, will depend on the specific licensing purchased. Underlying Altium Designer is the DXP integration platform which brings together Altium Designer's various editors and software engines, and provides a consistent user-interface across all the tools and editors. 143 APPENDIX C The Altium Designer environment is fully customizable, allowing you to set up the workspace to suit the way you work. A consistent selection and editing paradigm across different editors allows you to easily and smoothly switch between various design tasks within the Altium Designer environment [38]. In Figure C.1 is summarizes some of the key elements of the Altium Designer environment. Figure C.1 - Altium Designer Software 144 APPENDIX D Appendix D Easy-Radio Software and Configuration Command Set The Easy-Radio modules are supplied with a programming software ER ver. 2.03 (the Easy radio web site www.easy-Radio.co.uk should be checked for updated software and registered users will be sent email notifications of available upgrades). The file name is ER V2_03.exe. This file no need for any Windows installation procedure. It has been tested on the following operating systems: Windows 95, Windows 98, Windows ME, Windows 2000 & Windows XP. The programme takes direct control of the PC Serial port (Com 1 - default) which must be present and not being used by any other application. A small file (Test.ini) is created on the Root drive. After opening the programme (double click on the exe file) the screen below will open and serial communications should be established with the Easy Radio module on the connected Demonstration Board for programming it. Figure D.1 – RS232 settings After the first setup windows, the software appear on the screen (see Figure D.2). This software allows the following parameters to be configured: UART Bound Rate, Power Level, Frequency, Power Saving, Other settings and other special test modes. 145 APPENDIX D Figure D.2 – Software Easy-Radio Each parameter may be configured by selecting the required value from the ‘drop down’ boxes and then clicking the ‘Update’ button. The ‘Terminal Window’ will then display the actual text command that has been sent to the Easy-Radio module and the module will ‘echo’ the command that has just been sent. If the ‘Auto ACK’ check box is ticked (as shown) the new setting will automatically and permanently saved in non-volatile memory within the module. If the check box is not ticked the ‘ACK’ button should be manually clicked after each and every modification. Figure D.3 – Settings Software Easy-Radio 146 APPENDIX D The programming software sends ‘Text Commands’ to the modules and this action can be performed by terminal software or the host’s Microcontroller using the following list of commands: 147 APPENDIX D To successfully send a command do the following: 1. Send Command from host: e.g. ER_CMD#U5 (Set UART BAUD to 38400) 2. In the case of a TRS/RS: a. Wait for echo of command from module. e.g. ER_CMD#U5 148 APPENDIX D In the case of a TS: b. Wait 20mS 3. Send the ASCII string from the host: ACK The commands should be sent exactly as shown (case sensitive) with no spaces between characters. The ACK command is sent as three ASCII characters, ACK in sequence. ‘A’’C’’K’ . Note that the TS (transmitter) devices send data ‘over air’ as they are not equipped with a serial data out or handshake pins. This takes approximately 20mS and time should be taken in to account before sending the ‘ACK’ sequence “FAST ACK” - In this mode the procedure to update settings is made much faster. In response to an ER_CMD#x string the TRS/RS module will reply with a single HEX 6 (0x06) which is the ASCII ACK value. The host will then issue the same single byte 0x06 in replacement of the Txt version of “ACK”. 149 BIBLIOGRAPHY Bibliography [1] L. Ginzkey and W. Zenk, “Conductivity observations in oceanography”, 1981 [2] “Electrolytic conductivity measurement - Theory & Application”, in Aquarius Technical Bulletin, No. 08, March, 2002. [3] United States Department of Agriculture's, “Measurement of Electroconductivity” in a The Agricultural Research Service (ARS), web site http://www.ars.usda.gov [4] “Electrical Conductivity”, in The Encyclopedia of Water, published by John Wiley and Sons, 2005. [5] “Conductivity Instrumentation”, in web site of the “DELTA OHM” company, http://www.deltaohm.com. 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